3-deoxy-3-fluoro-1,2-O-isopropylidene-4-O-benzoyl-5-thio-α-D-xylopyranose

Base Information

Chemical Name:3-deoxy-3-fluoro-1,2-O-isopropylidene-4-O-benzoyl-5-thio-α-D-xylopyranose
CAS No.:1333223-15-6
Molecular Formula:C₁₅H₁₇FO₄S
Molecular Weight:312.362
Hs Code.:

Synonyms:3-deoxy-3-fluoro-1,2-O-isopropylidene-4-O-benzoyl-5-thio-α-D-xylopyranose

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Chemical Property of 3-deoxy-3-fluoro-1,2-O-isopropylidene-4-O-benzoyl-5-thio-α-D-xylopyranose

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Technology Process of 3-deoxy-3-fluoro-1,2-O-isopropylidene-4-O-benzoyl-5-thio-α-D-xylopyranose

There total 3 articles about 3-deoxy-3-fluoro-1,2-O-isopropylidene-4-O-benzoyl-5-thio-α-D-xylopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1333223-08-7
3-deoxy-3-fluoro-1,2-O-isopropylidene-5-thio-α-D-xylopyranose

: 98-88-4
benzoyl chloride

: 1333223-15-6
3-deoxy-3-fluoro-1,2-O-isopropylidene-4-O-benzoyl-5-thio-α-D-xylopyranose

Guidance literature:: In pyridine; at 20 ℃; for 1h;
DOI:10.1016/j.carres.2011.05.013

Reference yield:

: 3-deoxy-3-fluoro-5-thio-D-xylopyranose

: 1333223-15-6
3-deoxy-3-fluoro-1,2-O-isopropylidene-4-O-benzoyl-5-thio-α-D-xylopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 20 h

2: pyridine / 1 h / 20 °C

With toluene-4-sulfonic acid; In pyridine; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2011.05.013

Reference yield:

: 3-deoxy-3-fluoro-5-S-acetyl-5-thio-D-xylofuranose

: 1333223-15-6
3-deoxy-3-fluoro-1,2-O-isopropylidene-4-O-benzoyl-5-thio-α-D-xylopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: ammonia / methanol / 2 h / 20 °C

2: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 20 h

3: pyridine / 1 h / 20 °C

With ammonia; toluene-4-sulfonic acid; In pyridine; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2011.05.013