N-Acetyl-N'-acetyl>-L-alanyl>hexane-1,6-diamine

Base Information

Chemical Name:N-Acetyl-N'-acetyl>-L-alanyl>hexane-1,6-diamine
CAS No.:145118-26-9
Molecular Formula:C₂₈H₃₆N₄O₄
Molecular Weight:492.618
Hs Code.:

N-Acetyl-N'-<N-<<4-(benzyloxy)-1H-indol-3-yl>acetyl>-L-alanyl>hexane-1,6-diamine

Synonyms:N-Acetyl-N'-acetyl>-L-alanyl>hexane-1,6-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Acetyl-N'-acetyl>-L-alanyl>hexane-1,6-diamine

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Technology Process of N-Acetyl-N'-acetyl>-L-alanyl>hexane-1,6-diamine

There total 6 articles about N-Acetyl-N'-acetyl>-L-alanyl>hexane-1,6-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.3%

: 145118-25-8
N-Acetyl-N'-(L-alanyl)hexane-1,6-diamine Hydrochloride

: 144923-56-8
4-Nitrophenyl <(4-Benzyloxy)-1H-indol-3-yl>acetate

: 145118-26-9
N-Acetyl-N'-acetyl>-L-alanyl>hexane-1,6-diamine

Guidance literature:: With triethylamine; In tetrahydrofuran; for 18h;
DOI:10.1002/hlca.19920750617

Reference yield:

: 1464-12-6
2-(4-(benzyloxy)-1H-indol-3-yl)acetic acid

: 145118-26-9
N-Acetyl-N'-acetyl>-L-alanyl>hexane-1,6-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 57.7 percent / N,N'-dicyclohexylcarbodiimide (DCC) / ethyl acetate / 1) ice-bath, 1 h, 2) r.t., 18 h

2: 94.3 percent / Et₃N / tetrahydrofuran / 18 h

With triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethyl acetate;
DOI:10.1002/hlca.19920750617

Reference yield:

: 65915-94-8
N-(tert-butoxycarbonyl)-1,6-diaminohexane hydrochloride

: 145118-26-9
N-Acetyl-N'-acetyl>-L-alanyl>hexane-1,6-diamine

Guidance literature:: Multi-step reaction with 5 steps

1: 74.3 percent / pyridine / CH₂Cl₂ / 1) 0 deg C, 1 h, 2) r.t., 24 h

2: 93.6 percent / HCl / dioxane / 1 h

3: 57.7 percent / Et₃N / tetrahydrofuran / 18 h / Ambient temperature; Irradiation

4: 91.1 percent / HCl / dioxane / 0.67 h

5: 94.3 percent / Et₃N / tetrahydrofuran / 18 h

With pyridine; hydrogenchloride; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1002/hlca.19920750617