(S)-1-benzyloxycarbonyl-4-tert-butyldimethylsilyloxy-1,2,3,4-tetrahydroquinoline

Base Information

Chemical Name:(S)-1-benzyloxycarbonyl-4-tert-butyldimethylsilyloxy-1,2,3,4-tetrahydroquinoline
CAS No.:934192-24-2
Molecular Formula:C₂₃H₃₁NO₃Si
Molecular Weight:397.59
Hs Code.:

Synonyms:(S)-1-benzyloxycarbonyl-4-tert-butyldimethylsilyloxy-1,2,3,4-tetrahydroquinoline

Suppliers and Price of (S)-1-benzyloxycarbonyl-4-tert-butyldimethylsilyloxy-1,2,3,4-tetrahydroquinoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-1-benzyloxycarbonyl-4-tert-butyldimethylsilyloxy-1,2,3,4-tetrahydroquinoline

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-1-benzyloxycarbonyl-4-tert-butyldimethylsilyloxy-1,2,3,4-tetrahydroquinoline

There total 6 articles about (S)-1-benzyloxycarbonyl-4-tert-butyldimethylsilyloxy-1,2,3,4-tetrahydroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.8%

: (S)-1-benzyloxycarbonyl-4-hydroxy-1,2,3,4-tetrahydroquinoline

: 18162-48-6
tert-butyldimethylsilyl chloride

: 934192-24-2
(S)-1-benzyloxycarbonyl-4-tert-butyldimethylsilyloxy-1,2,3,4-tetrahydroquinoline

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

Reference yield:

: 108-05-4,9003-20-7
vinyl acetate

: 1-benzyloxycarbonyl-4-hydroxy-1,2,3,4-tetrahydroquinoline

: 18162-48-6
tert-butyldimethylsilyl chloride

: 934192-24-2
(S)-1-benzyloxycarbonyl-4-tert-butyldimethylsilyloxy-1,2,3,4-tetrahydroquinoline

Guidance literature:: vinyl acetate; 1-benzyloxycarbonyl-4-hydroxy-1,2,3,4-tetrahydroquinoline; In ethyl acetate; at 30 ℃; for 18h; Enzymatic reaction;

tert-butyldimethylsilyl chloride; With 1H-imidazole; In N,N-dimethyl-formamide; at 40 ℃; for 0.6h; Further stages;

Reference yield:

: 108-05-4,9003-20-7
vinyl acetate

: 1-benzyloxycarbonyl-4-hydroxy-1,2,3,4-tetrahydroquinoline

: 18162-48-6
tert-butyldimethylsilyl chloride

: 934192-24-2
(S)-1-benzyloxycarbonyl-4-tert-butyldimethylsilyloxy-1,2,3,4-tetrahydroquinoline

: (R)-1-benzyloxycarbonyl-4-hydroxy-1,2,3,4-tetrahydroquinoline

Guidance literature:: vinyl acetate; 1-benzyloxycarbonyl-4-hydroxy-1,2,3,4-tetrahydroquinoline; In ethyl acetate; at 30 ℃; for 18h; Enzymatic reaction;

tert-butyldimethylsilyl chloride; With 1H-imidazole; In N,N-dimethyl-formamide; at 40 ℃; for 0.6h;

With methanol; potassium carbonate; In methanol; at 50 ℃; for 0.00333333h; Overall yield = 2.25 g;