tert-butyldimethylsilyl 3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranoside

Base Information

Chemical Name:tert-butyldimethylsilyl 3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranoside
CAS No.:1129426-97-6
Molecular Formula:C₃₉H₄₉NO₇Si
Molecular Weight:671.906
Hs Code.:

Synonyms:tert-butyldimethylsilyl 3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyldimethylsilyl 3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranoside

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Technology Process of tert-butyldimethylsilyl 3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranoside

There total 2 articles about tert-butyldimethylsilyl 3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 81927-55-1
O-benzyl 2,2,2-trichloroacetimidate

: 216877-35-9
tert-butyldimethylsilyl 2-deoxy-2-dimethylmaleoyl-β-D-glucopyranoside

: 1129426-97-6
tert-butyldimethylsilyl 3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranoside

Guidance literature:: O-benzyl 2,2,2-trichloroacetimidate; tert-butyldimethylsilyl 2-deoxy-2-dimethylmaleoyl-β-D-glucopyranoside; In hexane; dichloromethane; at 20 ℃; for 0.5h; Molecular sieve; Inert] atmosphere;

With trifluorormethanesulfonic acid; In hexane; dichloromethane; Cooling with ice; Inwert atmosphere;

Reference yield: 25.0%

: 100-39-0
benzyl bromide

: 216877-35-9
tert-butyldimethylsilyl 2-deoxy-2-dimethylmaleoyl-β-D-glucopyranoside

: 1129426-89-6
3-(dibenzylamino)butanenitrile

: 1129426-97-6
tert-butyldimethylsilyl 3,4,6-tri-O-benzyl-2-dimethylmaleimido-2-deoxy-β-D-glycopyranoside

: 72687-57-1
β-benzylamino-butyronitrile

: 645-59-0
dihydrocinnamonitrile

Guidance literature:: tert-butyldimethylsilyl 2-deoxy-2-dimethylmaleoyl-β-D-glucopyranoside; With sodium hydride; In acetonitrile; mineral oil; at 20 ℃; for 0.5h; Inert atmosphere;

benzyl bromide; In acetonitrile; mineral oil; at 20 - 35 ℃; Inert atmosphere;