6-methyl-3-(1-methylhydrazino)-5-oxo-4-thriphenylphosphoranylideneamino-4,5-dihydro<1,2,4>triazine

Base Information

• Chemical Name: 6-methyl-3-(1-methylhydrazino)-5-oxo-4-thriphenylphosphoranylideneamino-4,5-dihydro<1,2,4>triazine
• CAS No.: 116471-24-0
• Molecular Formula: C₂₃H₂₃N₆OP
• Molecular Weight: 430.449

Synonyms:6-methyl-3-(1-methylhydrazino)-5-oxo-4-thriphenylphosphoranylideneamino-4,5-dihydro<1,2,4>triazine

Chemical Property of 6-methyl-3-(1-methylhydrazino)-5-oxo-4-thriphenylphosphoranylideneamino-4,5-dihydro<1,2,4>triazine

Chemical Property:

Purity/Quality:

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Technology Process of 6-methyl-3-(1-methylhydrazino)-5-oxo-4-thriphenylphosphoranylideneamino-4,5-dihydro<1,2,4>triazine

There total 1 articles about 6-methyl-3-(1-methylhydrazino)-5-oxo-4-thriphenylphosphoranylideneamino-4,5-dihydro<1,2,4>triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-amino-6-methyl-3-(1-methylhydrazino)-5-oxo-4,5-dihydro<1,2,4>triazine (116471-23-9) + triphenylphosphine (603-35-0) → 6-methyl-3-(1-methylhydrazino)-5-oxo-4-thriphenylphosphoranylideneamino-4,5-dihydro<1,2,4>triazine (116471-24-0)

Guidance literature:

With bromine; triethylamine; Yield given. Multistep reaction; 1.) benzene, 0-5 deg C, 1 h, 2.) benzene, reflux, 24 h;

DOI:10.1016/S0040-4020(01)81733-6

Reference yield: 67.0%

6-methyl-3-(1-methylhydrazino)-5-oxo-4-thriphenylphosphoranylideneamino-4,5-dihydro<1,2,4>triazine (116471-24-0) + 4-methoxy-benzoyl chloride (100-07-2) → 6-methyl-3-<1-methyl-2-(p-methoxybenzoyl)hydrazino>-5-oxo-4-triphenylphosphoranylideneamino-4,5-dihydro<1,2,4>triazine (116471-25-1)

Guidance literature:

With triethylamine; In benzene; Ambient temperature;

DOI:10.1039/P19890000247

Reference yield: 64.0%

6-methyl-3-(1-methylhydrazino)-5-oxo-4-thriphenylphosphoranylideneamino-4,5-dihydro<1,2,4>triazine (116471-24-0) + 4-methoxy-benzoyl chloride (100-07-2) → 3-(p-methoxyphenyl)-1,4-dihydro-1,7-dimethyl-6-oxo-4H-<1,2,4>triazino<4,3-b><1,2,4,5>tetrazine (116471-39-7)

Guidance literature:

With triethylamine; In benzene; for 6h; Heating;

DOI:10.1016/S0040-4020(01)81733-6

upstream raw materials:

4-amino-6-methyl-3-(1-methylhydrazino)-5-oxo-4,5-dihydro<1,2,4>triazine

triphenylphosphine

Downstream raw materials:

3-(2-benzylidene-1-methylhydrazino)-6-methyl-5-oxo-4-triphenylphosphoranylideneamino-4,5-dihydro<1,2,4>triazine

3-phenyl-1,4-dihydro-1,7-dimethyl-6-oxo-4H-<1,2,4>triazino<4,3-b><1,2,4,5>tetrazine

C₃₁H₂₉N₆O₂P

3-(p-tolyl)-1,4-dihydro-1,7-dimethyl-6-oxo-4H-<1,2,4>triazino<4,3-b><1,2,4,5>tetrazine

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