(1S)-1,6-dideoxy-1-[4-methoxy-3-(trans-4-n-propylcyclohexyl)methylphenyl]-D-glucopyranose

Base Information

Chemical Name:(1S)-1,6-dideoxy-1-[4-methoxy-3-(trans-4-n-propylcyclohexyl)methylphenyl]-D-glucopyranose
CAS No.:1431771-67-3
Molecular Formula:C₂₃H₃₆O₅
Molecular Weight:392.536
Hs Code.:

Synonyms:(1S)-1,6-dideoxy-1-[4-methoxy-3-(trans-4-n-propylcyclohexyl)methylphenyl]-D-glucopyranose

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Chemical Property of (1S)-1,6-dideoxy-1-[4-methoxy-3-(trans-4-n-propylcyclohexyl)methylphenyl]-D-glucopyranose

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Technology Process of (1S)-1,6-dideoxy-1-[4-methoxy-3-(trans-4-n-propylcyclohexyl)methylphenyl]-D-glucopyranose

There total 9 articles about (1S)-1,6-dideoxy-1-[4-methoxy-3-(trans-4-n-propylcyclohexyl)methylphenyl]-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1431771-89-9
C₂₉H₄₂O₈

: 1431771-67-3
(1S)-1,6-dideoxy-1-[4-methoxy-3-(trans-4-n-propylcyclohexyl)methylphenyl]-D-glucopyranose

Guidance literature:: With sodium; In methanol; at 20 ℃; for 1h;
DOI:10.1016/j.cclet.2013.03.026

Reference yield:

: C₄₄H₅₄O₅

: 1431771-67-3
(1S)-1,6-dideoxy-1-[4-methoxy-3-(trans-4-n-propylcyclohexyl)methylphenyl]-D-glucopyranose

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 1318910-22-3
1-deoxy-1-{4-methoxy-3-[(trans-4-n-propylcyclohexyl)methyl]phenyl}-β-D-glucose

: 1431771-67-3
(1S)-1,6-dideoxy-1-[4-methoxy-3-(trans-4-n-propylcyclohexyl)methylphenyl]-D-glucopyranose

Guidance literature:: Multi-step reaction with 6 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C

2: dmap / pyridine / 0 - 20 °C

3: acetic acid / water / 45 °C

4: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 20 °C

5: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 20 °C

6: sodium / methanol / 1 h / 20 °C

With 1H-imidazole; dmap; 2,2'-azobis(isobutyronitrile); iodine; tri-n-butyl-tin hydride; sodium; acetic acid; triphenylphosphine; In pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.cclet.2013.03.026