1-deoxy-1-{4-methoxy-3-[(trans-4-n-propylcyclohexyl)methyl]phenyl}-β-D-glucose

Base Information

Chemical Name:1-deoxy-1-{4-methoxy-3-[(trans-4-n-propylcyclohexyl)methyl]phenyl}-β-D-glucose
CAS No.:1318910-22-3
Molecular Formula:C₂₃H₃₆O₆
Molecular Weight:408.535
Hs Code.:

Synonyms:1-deoxy-1-{4-methoxy-3-[(trans-4-n-propylcyclohexyl)methyl]phenyl}-β-D-glucose

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Chemical Property of 1-deoxy-1-{4-methoxy-3-[(trans-4-n-propylcyclohexyl)methyl]phenyl}-β-D-glucose

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Technology Process of 1-deoxy-1-{4-methoxy-3-[(trans-4-n-propylcyclohexyl)methyl]phenyl}-β-D-glucose

There total 11 articles about 1-deoxy-1-{4-methoxy-3-[(trans-4-n-propylcyclohexyl)methyl]phenyl}-β-D-glucose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 2,3,4,6-tetra-O-acetyl-1-deoxy-1-{4-methoxy-3-[(trans-4-n-propylcyclohexyl)methyl]phenyl}-β-D-glucose

: 1318910-22-3
1-deoxy-1-{4-methoxy-3-[(trans-4-n-propylcyclohexyl)methyl]phenyl}-β-D-glucose

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 3h;

Reference yield: 87.0%

: 1-deoxy-1-{4-hydroxy-3-[(trans-4-n-propylcyclohexyl)methyl]phenyl}-β-D-glucose

: 74-88-4
methyl iodide

: 1318910-22-3
1-deoxy-1-{4-methoxy-3-[(trans-4-n-propylcyclohexyl)methyl]phenyl}-β-D-glucose

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 2,3,4,6-tetra-O-acetyl-1-{4-benzyloxy-3-[(trans-4-n-propylcyclohexyl)methyl]phenyl}-1-deoxy-β-D-glucose

: 1318910-22-3
1-deoxy-1-{4-methoxy-3-[(trans-4-n-propylcyclohexyl)methyl]phenyl}-β-D-glucose

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; palladium 10% on activated carbon / tetrahydrofuran / 5 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

3: sodium methylate / methanol / 3 h / 20 °C

With palladium 10% on activated carbon; hydrogen; sodium methylate; potassium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;