Technology Process of 2-O-Benzyl-3-O-palmitoyl-D-glycerinaldehyd
There total 7 articles about 2-O-Benzyl-3-O-palmitoyl-D-glycerinaldehyd which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 84.6 percent / DMAP, DCC / CH2Cl2 / Ambient temperature
2: 70 percent / TFA, 70percent aq. HClo4 / CH2Cl2 / 0.17 h / 0 - 5 °C
3: Pb(OAc)4 / ethyl acetate / 4 h / Ambient temperature
With
lead(IV) acetate; dmap; perchloric acid; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
dichloromethane; ethyl acetate;
DOI:10.1016/S0957-4166(97)00005-0
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 84.6 percent / DMAP, DCC / CH2Cl2 / Ambient temperature
2: 70 percent / TFA, 70percent aq. HClo4 / CH2Cl2 / 0.17 h / 0 - 5 °C
3: Pb(OAc)4 / ethyl acetate / 4 h / Ambient temperature
With
lead(IV) acetate; dmap; perchloric acid; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
dichloromethane; ethyl acetate;
DOI:10.1016/S0957-4166(97)00005-0
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 70 percent / TFA, 70percent aq. HClo4 / CH2Cl2 / 0.17 h / 0 - 5 °C
2: Pb(OAc)4 / ethyl acetate / 4 h / Ambient temperature
With
lead(IV) acetate; perchloric acid; trifluoroacetic acid;
In
dichloromethane; ethyl acetate;
DOI:10.1016/S0957-4166(97)00005-0