(2S,3R,5R)-3-Azido-2-hydroxy-5-(α-D-arabinofuranosyloxy)cyclohexanone O-benzyl oxime

Base Information

Chemical Name:(2S,3R,5R)-3-Azido-2-hydroxy-5-(α-D-arabinofuranosyloxy)cyclohexanone O-benzyl oxime
CAS No.:171074-33-2
Molecular Formula:C₁₈H₂₄N₄O₇
Molecular Weight:408.411
Hs Code.:

Synonyms:(2S,3R,5R)-3-Azido-2-hydroxy-5-(α-D-arabinofuranosyloxy)cyclohexanone O-benzyl oxime

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Chemical Property of (2S,3R,5R)-3-Azido-2-hydroxy-5-(α-D-arabinofuranosyloxy)cyclohexanone O-benzyl oxime

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Technology Process of (2S,3R,5R)-3-Azido-2-hydroxy-5-(α-D-arabinofuranosyloxy)cyclohexanone O-benzyl oxime

There total 6 articles about (2S,3R,5R)-3-Azido-2-hydroxy-5-(α-D-arabinofuranosyloxy)cyclohexanone O-benzyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 171074-32-1
(2S,3R,5R)-3-Azido-2-benzoyloxy-5-(2',3',5'-tri-O-benzoyl-α-D-arabinofuranosyloxy)cyclohexanone O-benzyl oxime

: 171074-33-2
(2S,3R,5R)-3-Azido-2-hydroxy-5-(α-D-arabinofuranosyloxy)cyclohexanone O-benzyl oxime

Guidance literature:: With sodium methylate; In methanol;
DOI:10.1016/0008-6215(95)00130-L

Reference yield:

: 171074-28-5
(2S,3R,5R)-3-Azido-2-benzoyloxy-5-hydroxycyclohexanone O-benzyl oxime

: 171074-33-2
(2S,3R,5R)-3-Azido-2-hydroxy-5-(α-D-arabinofuranosyloxy)cyclohexanone O-benzyl oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / HgBr₂, 4 A molecular sieves / CH₂Cl₂

2: 100 percent / NaOCH₃ / methanol

With 4 A molecular sieve; sodium methylate; mercury dibromide; In methanol; dichloromethane;
DOI:10.1016/0008-6215(95)00130-L

Reference yield:

: 4348-68-9
2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl bromide

: 171074-33-2
(2S,3R,5R)-3-Azido-2-hydroxy-5-(α-D-arabinofuranosyloxy)cyclohexanone O-benzyl oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / HgBr₂, 4 A molecular sieves / CH₂Cl₂

2: 100 percent / NaOCH₃ / methanol

With 4 A molecular sieve; sodium methylate; mercury dibromide; In methanol; dichloromethane;
DOI:10.1016/0008-6215(95)00130-L