C₂₀H₂₂OSi

Base Information

Chemical Name:C₂₀H₂₂OSi
CAS No.:1555881-02-1
Molecular Formula:C₂₀H₂₂OSi
Molecular Weight:306.48
Hs Code.:

Synonyms:C₂₀H₂₂OSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₂₂OSi

Chemical Property:

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Technology Process of C₂₀H₂₂OSi

There total 3 articles about C₂₀H₂₂OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S,S)-cis EZ-CrotylMix

: 1555880-99-3
C₁₉H₂₂O₂Si

: 1555881-02-1
C₂₀H₂₂OSi

Guidance literature:: (S,S)-cis EZ-CrotylMix; C₁₉H₂₂O₂Si; With scandium tris(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 1.5h; Inert atmosphere;

With tetrabutyl ammonium fluoride; In dichloromethane; water; for 1h; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol500051e

Reference yield:

: 1631-83-0
diphenylsilyl chloride

: 1555881-02-1
C₂₀H₂₂OSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

2.1: Rh(acac)(CO)₂ / benzene / 5 h / 20 °C / 15514.9 Torr / Autoclave

3.1: scandium tris(trifluoromethanesulfonate) / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

3.2: 1 h / Inert atmosphere

With Rh(acac)(CO)₂; triethylamine; scandium tris(trifluoromethanesulfonate); In dichloromethane; benzene;
DOI:10.1021/ol500051e

Reference yield:

: 40391-86-4
diphenyl(isopropoxy)silane

: 1555881-02-1
C₂₀H₂₂OSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: Rh(acac)(CO)₂ / benzene / 5 h / 20 °C / 15514.9 Torr / Autoclave

2.1: scandium tris(trifluoromethanesulfonate) / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere

With Rh(acac)(CO)₂; scandium tris(trifluoromethanesulfonate); In dichloromethane; benzene;
DOI:10.1021/ol500051e