(1S,2R,3R,4R,6R)-3-(tert-Butyl-dimethyl-silanyloxy)-6-methoxymethoxy-4-methoxymethyl-cyclohexane-1,2-diol

Base Information

Chemical Name:(1S,2R,3R,4R,6R)-3-(tert-Butyl-dimethyl-silanyloxy)-6-methoxymethoxy-4-methoxymethyl-cyclohexane-1,2-diol
CAS No.:868593-24-2
Molecular Formula:C₁₆H₃₄O₆Si
Molecular Weight:350.528
Hs Code.:

Synonyms:(1S,2R,3R,4R,6R)-3-(tert-Butyl-dimethyl-silanyloxy)-6-methoxymethoxy-4-methoxymethyl-cyclohexane-1,2-diol

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Chemical Property of (1S,2R,3R,4R,6R)-3-(tert-Butyl-dimethyl-silanyloxy)-6-methoxymethoxy-4-methoxymethyl-cyclohexane-1,2-diol

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Technology Process of (1S,2R,3R,4R,6R)-3-(tert-Butyl-dimethyl-silanyloxy)-6-methoxymethoxy-4-methoxymethyl-cyclohexane-1,2-diol

There total 7 articles about (1S,2R,3R,4R,6R)-3-(tert-Butyl-dimethyl-silanyloxy)-6-methoxymethoxy-4-methoxymethyl-cyclohexane-1,2-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 868593-22-0
C₂₂H₄₂O₆Si

: 868593-24-2
(1S,2R,3R,4R,6R)-3-(tert-Butyl-dimethyl-silanyloxy)-6-methoxymethoxy-4-methoxymethyl-cyclohexane-1,2-diol

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 20 ℃;
DOI:10.1055/s-2005-872222

Reference yield:

: 868593-19-5
C₁₅H₂₄O₅

: 868593-24-2
(1S,2R,3R,4R,6R)-3-(tert-Butyl-dimethyl-silanyloxy)-6-methoxymethoxy-4-methoxymethyl-cyclohexane-1,2-diol

Guidance literature:: Multi-step reaction with 4 steps

1.1: 87 percent / NaH / tetrahydrofuran; dimethylformamide

2.1: BH₃*SMe₂ / -20 °C

2.2: 92 percent / NaBO₃*4H₂O / tetrahydrofuran

3.1: 90 percent / imidazole / dimethylformamide

4.1: 90 percent / TsOH / methanol / 20 °C

With 1H-imidazole; dimethylsulfide borane complex; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1055/s-2005-872222

Reference yield:

: 868593-20-8
C₁₆H₂₆O₅

: 868593-24-2
(1S,2R,3R,4R,6R)-3-(tert-Butyl-dimethyl-silanyloxy)-6-methoxymethoxy-4-methoxymethyl-cyclohexane-1,2-diol

Guidance literature:: Multi-step reaction with 3 steps

1.1: BH₃*SMe₂ / -20 °C

1.2: 92 percent / NaBO₃*4H₂O / tetrahydrofuran

2.1: 90 percent / imidazole / dimethylformamide

3.1: 90 percent / TsOH / methanol / 20 °C

With 1H-imidazole; dimethylsulfide borane complex; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1055/s-2005-872222