(5aS,6R,9S,9aR)-5a,6,7,8,9,9a-Hexahydro-6,11,11-triMethyl-2-(2,4,6-triMethylphenyl)-6,9-Methano-4H-[1,2,4]triazolo[3,4-c][1,4]benzoxaziniuM tetrafluoroborate

Base Information

• Chemical Name: (5aS,6R,9S,9aR)-5a,6,7,8,9,9a-Hexahydro-6,11,11-triMethyl-2-(2,4,6-triMethylphenyl)-6,9-Methano-4H-[1,2,4]triazolo[3,4-c][1,4]benzoxaziniuM tetrafluoroborate
• CAS No.: 1037287-79-8
• Molecular Formula: BF₄*C₂₂H₃₀N₃O
• Molecular Weight: 439.304
• Mol file: 1037287-79-8.mol

Synonyms:BF₄^(1-)*C₂₂H₃₀N₃O⁽¹⁺⁾

Chemical Property of (5aS,6R,9S,9aR)-5a,6,7,8,9,9a-Hexahydro-6,11,11-triMethyl-2-(2,4,6-triMethylphenyl)-6,9-Methano-4H-[1,2,4]triazolo[3,4-c][1,4]benzoxaziniuM tetrafluoroborate

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

(5aS,6R,9S,9aR)-5a,6,7,8,9,9a-Hexahydro-6,11,11-trimethyl-2-(2,4,6-trimethylphenyl)-6,9-methano-4H-[1,2,4]triazolo[3,4-c][1,4]benzoxazinium tetrafluoroborate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (5aS,6R,9S,9aR)-5a,6,7,8,9,9a-Hexahydro-6,11,11-triMethyl-2-(2,4,6-triMethylphenyl)-6,9-Methano-4H-[1,2,4]triazolo[3,4-c][1,4]benzoxaziniuM tetrafluoroborate

There total 1 articles about (5aS,6R,9S,9aR)-5a,6,7,8,9,9a-Hexahydro-6,11,11-triMethyl-2-(2,4,6-triMethylphenyl)-6,9-Methano-4H-[1,2,4]triazolo[3,4-c][1,4]benzoxaziniuM tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

(1R,2S,7R,8S)-(+)-1,11,11-trimethyl-3-oxa-6-aza-tricyclo-[6.2.1.0(2,7)]undecan-5-one (1037287-73-2) + trimethoxonium tetrafluoroborate (420-37-1) + 2,4,6-trimethylphenylhydrazine (13636-54-9) → BF4(1-)*C22H30N3O(1+) (1037287-79-8)

Guidance literature:

(1R,2S,7R,8S)-(+)-1,11,11-trimethyl-3-oxa-6-aza-tricyclo-[6.2.1.0(2,7)]undecan-5-one; trimethoxonium tetrafluoroborate; In dichloromethane; at 20 ℃; for 24h;

2,4,6-trimethylphenylhydrazine; In dichloromethane; at 20 ℃; for 24h;

With orthoformic acid triethyl ester; In chlorobenzene; at 110 ℃; for 72h; Further stages.;

DOI:10.1039/b801004h

Reference yield: 44.0%

bis(1,5-cyclooctadiene)diiridium(I) dichloride (12112-67-3) + BF4(1-)*C22H30N3O(1+) (1037287-79-8) → C30H41ClIrN3O

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.3987/COM-16-S(S)19

upstream raw materials:

(1R,2S,7R,8S)-(+)-1,11,11-trimethyl-3-oxa-6-aza-tricyclo-[6.2.1.0(2,7)]undecan-5-one

trimethoxonium tetrafluoroborate

2,4,6-trimethylphenylhydrazine

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1037287-79-8 (5aS,6R,9S,9aR)-5a,6,7,8,9,9a-Hexahydro-6,11,11-triMethyl-2-(2,4,6-triMethylphenyl)-6,9-Methano-4H-[1,2,4]triazolo[3,4-c][1,4]benzoxaziniuM tetrafluoroborate

Send

Send

Metric Ton KG G Pound L ML

Send

Send