bispyridine-2,6-dicarboxamide

Base Information

Chemical Name:bispyridine-2,6-dicarboxamide
CAS No.:218143-47-6
Molecular Formula:C₂₅H₂₅N₅O₈
Molecular Weight:523.502
Hs Code.:

bis<N-ethyl-N-(4-methoxy-2-nitrophenyl)>pyridine-2,6-dicarboxamide

Synonyms:bispyridine-2,6-dicarboxamide

Suppliers and Price of bispyridine-2,6-dicarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bispyridine-2,6-dicarboxamide

Chemical Property:

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Technology Process of bispyridine-2,6-dicarboxamide

There total 3 articles about bispyridine-2,6-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 3739-94-4
2,6-Pyridinedicarbonyl dichloride

: 3360-85-8
N-ethyl-(4-methoxy-2-nitrophenyl)amine

: 218143-47-6
bispyridine-2,6-dicarboxamide

Guidance literature:: With triethylamine; In dichloromethane; for 8h; Heating;
DOI:10.1021/ja982545n

Reference yield:

: 10298-80-3
2-chloro-5-methoxynitrobenzene

: 218143-47-6
bispyridine-2,6-dicarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / H₂O / 12 h / 100 °C

2: 75 percent / Et₃N / CH₂Cl₂ / 8 h / Heating

With triethylamine; In dichloromethane; water;
DOI:10.1021/ja982545n

Reference yield:

: 499-83-2
Pyridine-2,6-dicarboxylic acid

: 218143-47-6
bispyridine-2,6-dicarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride, DMF / 0.75 h / Heating

2: 75 percent / Et₃N / CH₂Cl₂ / 8 h / Heating

With thionyl chloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/ja982545n