3-(((benzyloxy)(2-(((benzyloxy)carbonyl)amino)ethoxy)phosphoryl)oxy)propane-1,2-diyl distearate

Base Information

Chemical Name:3-(((benzyloxy)(2-(((benzyloxy)carbonyl)amino)ethoxy)phosphoryl)oxy)propane-1,2-diyl distearate
CAS No.:121075-80-7
Molecular Formula:C₅₆H₉₄NO₁₀P
Molecular Weight:972.337
Hs Code.:

Synonyms:3-(((benzyloxy)(2-(((benzyloxy)carbonyl)amino)ethoxy)phosphoryl)oxy)propane-1,2-diyl distearate

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Chemical Property of 3-(((benzyloxy)(2-(((benzyloxy)carbonyl)amino)ethoxy)phosphoryl)oxy)propane-1,2-diyl distearate

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Technology Process of 3-(((benzyloxy)(2-(((benzyloxy)carbonyl)amino)ethoxy)phosphoryl)oxy)propane-1,2-diyl distearate

There total 6 articles about 3-(((benzyloxy)(2-(((benzyloxy)carbonyl)amino)ethoxy)phosphoryl)oxy)propane-1,2-diyl distearate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: benzyl (2-(((benzyloxy)(2,3-dihydroxypropoxy)phosphoryl)oxy)ethyl)carbamate

: 57-11-4
stearic acid

: 121075-80-7
3-(((benzyloxy)(2-(((benzyloxy)carbonyl)amino)ethoxy)phosphoryl)oxy)propane-1,2-diyl distearate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1055/a-1516-9893

Reference yield:

: benzyl (2-(((benzyloxy)(2,3-bis((tert-butyldimethylsilyl)oxy)propoxy)phosphoryl)oxy)ethyl)carbamate

: 121075-80-7
3-(((benzyloxy)(2-(((benzyloxy)carbonyl)amino)ethoxy)phosphoryl)oxy)propane-1,2-diyl distearate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogen sulfate / acetonitrile; water / 6 h / 0 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 h / 20 °C / Inert atmosphere

With dmap; sodium hydrogen sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; water; acetonitrile;
DOI:10.1055/a-1516-9893

Reference yield:

: 77987-49-6
benzyl 2-hydroxyethylcarbamate

: 121075-80-7
3-(((benzyloxy)(2-(((benzyloxy)carbonyl)amino)ethoxy)phosphoryl)oxy)propane-1,2-diyl distearate

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 5 h / 0 - 20 °C / Inert atmosphere

2.1: lithium tert-butoxide / toluene; hexane / 1 h / 0 °C / Inert atmosphere

2.2: 3 h / -45 °C

3.1: lithium tert-butoxide / toluene; hexane / 1 h / 0 °C / Inert atmosphere

3.2: 12 h / 20 °C / Inert atmosphere

4.1: sodium hydrogen sulfate / acetonitrile; water / 6 h / 0 °C

5.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 h / 20 °C / Inert atmosphere

With dmap; sodium hydrogen sulfate; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium tert-butoxide; In hexane; dichloromethane; water; toluene; acetonitrile;
DOI:10.1055/a-1516-9893