9-<3-deoxy-5-O-(4-methoxytrityl)-2-O-methylsulfonyl-β-D-threo-pentofuranosyl>hypoxanthine

Base Information

Chemical Name:9-<3-deoxy-5-O-(4-methoxytrityl)-2-O-methylsulfonyl-β-D-threo-pentofuranosyl>hypoxanthine
CAS No.:140679-81-8
Molecular Formula:C₃₁H₃₀N₄O₇S
Molecular Weight:602.668
Hs Code.:

Synonyms:9-<3-deoxy-5-O-(4-methoxytrityl)-2-O-methylsulfonyl-β-D-threo-pentofuranosyl>hypoxanthine

Suppliers and Price of 9-<3-deoxy-5-O-(4-methoxytrityl)-2-O-methylsulfonyl-β-D-threo-pentofuranosyl>hypoxanthine

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Chemical Property of 9-<3-deoxy-5-O-(4-methoxytrityl)-2-O-methylsulfonyl-β-D-threo-pentofuranosyl>hypoxanthine

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Technology Process of 9-<3-deoxy-5-O-(4-methoxytrityl)-2-O-methylsulfonyl-β-D-threo-pentofuranosyl>hypoxanthine

There total 7 articles about 9-<3-deoxy-5-O-(4-methoxytrityl)-2-O-methylsulfonyl-β-D-threo-pentofuranosyl>hypoxanthine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69659-63-8
5'-O-(4-methoxytrityl)inosine

: 140679-81-8
9-<3-deoxy-5-O-(4-methoxytrityl)-2-O-methylsulfonyl-β-D-threo-pentofuranosyl>hypoxanthine

Guidance literature:: Multi-step reaction with 3 steps

1: 1) pyridine / 1) RT, 70 min, 2) 4h, RT

2: 89 percent / KOH, NaBH₄ / methanol; benzene / 27.5 h / Ambient temperature

3: 1) pyridine, 2) KOH / 1a) 0 to 5 deg C, 5 min, 1b) RT, 2.7h, 2) MeOH, 0 to 5 deg C, 8 min

With pyridine; potassium hydroxide; sodium tetrahydroborate; In methanol; benzene;
DOI:10.1039/P19920000469

Reference yield:

: 58-63-9
Inosine

: 140679-81-8
9-<3-deoxy-5-O-(4-methoxytrityl)-2-O-methylsulfonyl-β-D-threo-pentofuranosyl>hypoxanthine

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / pyridine / dimethylsulfoxide / 19 h

2: 1) pyridine / 1) RT, 70 min, 2) 4h, RT

3: 89 percent / KOH, NaBH₄ / methanol; benzene / 27.5 h / Ambient temperature

4: 1) pyridine, 2) KOH / 1a) 0 to 5 deg C, 5 min, 1b) RT, 2.7h, 2) MeOH, 0 to 5 deg C, 8 min

With pyridine; potassium hydroxide; sodium tetrahydroborate; In methanol; dimethyl sulfoxide; benzene;
DOI:10.1039/P19920000469

Reference yield:

: 14470-28-1
mono-4-methoxytrityl chloride

: 140679-81-8
9-<3-deoxy-5-O-(4-methoxytrityl)-2-O-methylsulfonyl-β-D-threo-pentofuranosyl>hypoxanthine

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / pyridine / dimethylsulfoxide / 19 h

2: 1) pyridine / 1) RT, 70 min, 2) 4h, RT

3: 89 percent / KOH, NaBH₄ / methanol; benzene / 27.5 h / Ambient temperature

4: 1) pyridine, 2) KOH / 1a) 0 to 5 deg C, 5 min, 1b) RT, 2.7h, 2) MeOH, 0 to 5 deg C, 8 min

With pyridine; potassium hydroxide; sodium tetrahydroborate; In methanol; dimethyl sulfoxide; benzene;
DOI:10.1039/P19920000469