ethyl (2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1→3)-2,4-di-O-benzyl-1-thio-α-L-rhamnopyranoside

Base Information

Chemical Name:ethyl (2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1→3)-2,4-di-O-benzyl-1-thio-α-L-rhamnopyranoside
CAS No.:1333325-36-2
Molecular Formula:C₄₉H₅₅N₃O₈S
Molecular Weight:846.057
Hs Code.:

Synonyms:ethyl (2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1→3)-2,4-di-O-benzyl-1-thio-α-L-rhamnopyranoside

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Chemical Property of ethyl (2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1→3)-2,4-di-O-benzyl-1-thio-α-L-rhamnopyranoside

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Technology Process of ethyl (2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1→3)-2,4-di-O-benzyl-1-thio-α-L-rhamnopyranoside

There total 1 articles about ethyl (2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1→3)-2,4-di-O-benzyl-1-thio-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1333325-34-0
ethyl (3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-glucopyranosyl)-(1→3)-2,4-di-O-benzyl-1-thio-α-L-rhamnopyranoside

: 100-39-0
benzyl bromide

: 1333325-36-2
ethyl (2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1→3)-2,4-di-O-benzyl-1-thio-α-L-rhamnopyranoside

Guidance literature:: With tetrabutylammomium bromide; sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.3762/bjoc.7.137

Reference yield: 82.0%

: 1333325-31-7
4-methoxyphenyl (2,3-di-O-acetyl-6-O-benzyl-α-D-glucopyranosyl)-(1→4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

: 1333325-36-2
ethyl (2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1→3)-2,4-di-O-benzyl-1-thio-α-L-rhamnopyranoside

: 4-methoxyphenyl (2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1→3)-(2,4-di-O-benzyl-β-L-rhamnopyranosyl)-(1→4)-(2,3-di-O-acetyl-6-O-benzyl-α-D-glucopyranosyl)-(1→4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

: 1333325-38-4
4-methoxyphenyl (2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1→3)-(2,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(2,3-di-O-acetyl-6-O-benzyl-α-D-glucopyranosyl)-(1→4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; perchloric acid adsorbed on silica gel; In dichloromethane; at -10 ℃; for 1h; stereoselective reaction; Molecular sieve;
DOI:10.3762/bjoc.7.137