2-(p-(beta-Ethyl-alpha-(p-methoxyphenyl)styryl)phenoxy)triethylamine

Base Information

• Chemical Name: 2-(p-(beta-Ethyl-alpha-(p-methoxyphenyl)styryl)phenoxy)triethylamine
• CAS No.: 35258-20-9
• Molecular Formula: C29H35NO2
• Molecular Weight: 429.5937
• Mol file: 35258-20-9.mol

Synonyms:BRN 2018226;2-(p-(beta-Ethyl-alpha-(p-methoxyphenyl)styryl)phenoxy)triethylamine;Triethylamine, 2-(p-(beta-ethyl-alpha-(p-methoxyphenyl)styryl)phenoxy)-;35258-20-9;LS-157337

Chemical Property of 2-(p-(beta-Ethyl-alpha-(p-methoxyphenyl)styryl)phenoxy)triethylamine

Chemical Property:

• Vapor Pressure: 7.52E-12mmHg at 25°C
• Boiling Point: 542.9°C at 760 mmHg
• Flash Point: 149.5°C
• Density: 1.039g/cm³
• XLogP3: 7.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 11
• Exact Mass: 429.266779359
• Heavy Atom Count: 32
• Complexity: 533

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC(=C(C1=CC=C(C=C1)OC)C2=CC=C(C=C2)OCCN(CC)CC)C3=CC=CC=C3
• Isomeric SMILES: CC/C(=C(\C1=CC=C(C=C1)OC)/C2=CC=C(C=C2)OCCN(CC)CC)/C3=CC=CC=C3

Technology Process of 2-(p-(beta-Ethyl-alpha-(p-methoxyphenyl)styryl)phenoxy)triethylamine

There total 3 articles about 2-(p-(beta-Ethyl-alpha-(p-methoxyphenyl)styryl)phenoxy)triethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(4-methoxyphenyl)-2-phenylbutan-1-one (78423-10-6) → Diethyl-(2-{4-[(Z)-1-(4-methoxy-phenyl)-2-phenyl-but-1-enyl]-phenoxy}-ethyl)-amine (35258-20-9)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine hydrochloride / Heating

2: (i) NaOEt, EtOH, (ii) /BRN= 605300/, benzene

3: (i) Mg, Et₂O, (ii) /BRN= 2005011/, (iii) aq. HCl, EtOH

With pyridine hydrochloride;

Reference yield:

1-(4'-hydroxyphenyl)-2-phenyl-n-butane-1-one (6966-21-8) → Diethyl-(2-{4-[(Z)-1-(4-methoxy-phenyl)-2-phenyl-but-1-enyl]-phenoxy}-ethyl)-amine (35258-20-9)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) NaOEt, EtOH, (ii) /BRN= 605300/, benzene

2: (i) Mg, Et₂O, (ii) /BRN= 2005011/, (iii) aq. HCl, EtOH

Reference yield:

1-bromo-4-methoxy-benzene (104-92-7) + 1-[4-(2-diethylamino-ethoxy)-phenyl]-2-phenyl-butan-1-one (74631-77-9) → Diethyl-(2-{4-[(Z)-1-(4-methoxy-phenyl)-2-phenyl-but-1-enyl]-phenoxy}-ethyl)-amine (35258-20-9)

Guidance literature:

Multistep reaction; (i) Mg, Et₂O, (ii) /BRN= 2005011/, (iii) aq. HCl, EtOH;

upstream raw materials:

1-bromo-4-methoxy-benzene

1-[4-(2-diethylamino-ethoxy)-phenyl]-2-phenyl-butan-1-one

1-(4-methoxyphenyl)-2-phenylbutan-1-one

1-(4'-hydroxyphenyl)-2-phenyl-n-butane-1-one