5-chloro-N-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenethyl)-2,4-dihydroxybenzamide

Base Information

Chemical Name:5-chloro-N-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenethyl)-2,4-dihydroxybenzamide
CAS No.:913622-30-7
Molecular Formula:C₂₁H₂₅ClN₂O₉
Molecular Weight:484.891
Hs Code.:

Synonyms:5-chloro-N-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenethyl)-2,4-dihydroxybenzamide

Suppliers and Price of 5-chloro-N-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenethyl)-2,4-dihydroxybenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-chloro-N-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenethyl)-2,4-dihydroxybenzamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-chloro-N-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenethyl)-2,4-dihydroxybenzamide

There total 5 articles about 5-chloro-N-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenethyl)-2,4-dihydroxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 913622-80-7
3-(2-azidoethyl)-2-methoxy-1,4-bis(methoxymethoxy)-5-nitrobenzene

: 913622-30-7
5-chloro-N-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenethyl)-2,4-dihydroxybenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 51 percent / sodium sulfide; Et₃N / methanol / 12 h

2: 63 percent / DCC / tetrahydrofuran / 12 h / 50 °C

3: H₂ / Pd/C / ethyl acetate / 48 h

4: 17.4 mg / CH₂Cl₂ / 12 h / 30 °C

With sodium sulfide; hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1021/jo061054f

Reference yield:

: 913622-27-2
2-(2-methoxy-3,6-bis(methoxymethoxy)-5-nitrophenyl)ethanamine

: 913622-30-7
5-chloro-N-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenethyl)-2,4-dihydroxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / DCC / tetrahydrofuran / 12 h / 50 °C

2: H₂ / Pd/C / ethyl acetate / 48 h

3: 17.4 mg / CH₂Cl₂ / 12 h / 30 °C

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1021/jo061054f

Reference yield:

: 912545-04-1
2,4-bis(benzyloxy)-5-chlorobenzoic acid

: 913622-30-7
5-chloro-N-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenethyl)-2,4-dihydroxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / DCC / tetrahydrofuran / 12 h / 50 °C

2: H₂ / Pd/C / ethyl acetate / 48 h

3: 17.4 mg / CH₂Cl₂ / 12 h / 30 °C

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1021/jo061054f