Technology Process of tris(triphenylstannyl)phosphine
There total 6 articles about tris(triphenylstannyl)phosphine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Ti(N(C(CH3)3)(3,5-C6H3(CH3)2)3;
In
benzene;
byproducts: ClTi(N(C(CH3)3)(3,5-C6H3(CH3)2)3; reaction at 20°C; isolated by repeated recrystn. from Et2O;
DOI:10.1039/c0nj00124d
- Guidance literature:
-
With
(4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; triethylamine;
In
acetonitrile;
at 20 ℃;
for 24h;
Reagent/catalyst;
Sealed tube;
Irradiation;
Schlenk technique;
Glovebox;
Inert atmosphere;
DOI:10.1002/anie.202110619
- Guidance literature:
-
With
1,3-dicyano-5-fluoro-2,4,6-tris(diphenylamino)benzene; Tetraphenyldiphosphin; diphenylphosphane; 1,3-bis-(bromomethyl)benzene;
In
acetonitrile; benzene;
for 24h;
Inert atmosphere;
Glovebox;
Sealed tube;
Irradiation;
DOI:10.1002/chem.202002646
