(R)-methyl 1-(2-(4-(2-(3,4-dihydroquinolin-1(2H)-yl)ethoxy)benzyl)hydrazinyl)-3,3-dimethyl-1-oxobutan-2-ylcarbamate

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Chemical Name:(R)-methyl 1-(2-(4-(2-(3,4-dihydroquinolin-1(2H)-yl)ethoxy)benzyl)hydrazinyl)-3,3-dimethyl-1-oxobutan-2-ylcarbamate
CAS No.:1313358-82-5
Molecular Formula:C₂₆H₃₆N₄O₄
Molecular Weight:468.596
Hs Code.:

Synonyms:(R)-methyl 1-(2-(4-(2-(3,4-dihydroquinolin-1(2H)-yl)ethoxy)benzyl)hydrazinyl)-3,3-dimethyl-1-oxobutan-2-ylcarbamate

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Chemical Property of (R)-methyl 1-(2-(4-(2-(3,4-dihydroquinolin-1(2H)-yl)ethoxy)benzyl)hydrazinyl)-3,3-dimethyl-1-oxobutan-2-ylcarbamate

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Technology Process of (R)-methyl 1-(2-(4-(2-(3,4-dihydroquinolin-1(2H)-yl)ethoxy)benzyl)hydrazinyl)-3,3-dimethyl-1-oxobutan-2-ylcarbamate

There total 8 articles about (R)-methyl 1-(2-(4-(2-(3,4-dihydroquinolin-1(2H)-yl)ethoxy)benzyl)hydrazinyl)-3,3-dimethyl-1-oxobutan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1313358-68-7
(R,Z)-methyl 1-(2-(4-(2-(3,4-dihydroquinolin-1(2H)-yl)ethoxy)benzylidene)hydrazinyl)-3,3-dimethyl-1-oxobutan-2-ylcarbamate

: 1313358-82-5
(R)-methyl 1-(2-(4-(2-(3,4-dihydroquinolin-1(2H)-yl)ethoxy)benzyl)hydrazinyl)-3,3-dimethyl-1-oxobutan-2-ylcarbamate

Guidance literature:: With hydrogen; palladium on carbon; In ethanol; at 20 ℃; for 18h; Inert atmosphere;

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1313358-82-5
(R)-methyl 1-(2-(4-(2-(3,4-dihydroquinolin-1(2H)-yl)ethoxy)benzyl)hydrazinyl)-3,3-dimethyl-1-oxobutan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 20 °C / Reflux

2: N,N-dimethyl-formamide / 12 h / 20 °C / Reflux

3: isopropyl alcohol / 16 h / 20 °C / Reflux

4: hydrogen / palladium on carbon / ethanol / 18 h / 20 °C / Inert atmosphere

With hydrogen; potassium carbonate; palladium on carbon; In ethanol; N,N-dimethyl-formamide; isopropyl alcohol; acetone;

Reference yield:

: 20859-02-3
L-tert-Leucine

: 1313358-82-5
(R)-methyl 1-(2-(4-(2-(3,4-dihydroquinolin-1(2H)-yl)ethoxy)benzyl)hydrazinyl)-3,3-dimethyl-1-oxobutan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / 1,4-dioxane; water / 18 h / 60 °C / pH 8 - 9

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; 4-methyl-morpholine / ethyl acetate / 0 °C

2.2: 18 h / 20 °C

3.1: hydrogenchloride; water / 1,4-dioxane / 12 h / 0 - 20 °C

4.1: isopropyl alcohol / 16 h / 20 °C / Reflux

5.1: hydrogen / palladium on carbon / ethanol / 18 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; palladium on carbon; In 1,4-dioxane; ethanol; water; ethyl acetate; isopropyl alcohol;