Phosphorous acid benzyl ester 2,3-bis-octyloxy-propyl ester methyl ester

Base Information

Chemical Name:Phosphorous acid benzyl ester 2,3-bis-octyloxy-propyl ester methyl ester
CAS No.:1028275-27-5
Molecular Formula:C₂₇H₄₉O₅P
Molecular Weight:484.657
Hs Code.:

Synonyms:Phosphorous acid benzyl ester 2,3-bis-octyloxy-propyl ester methyl ester

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Chemical Property of Phosphorous acid benzyl ester 2,3-bis-octyloxy-propyl ester methyl ester

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Technology Process of Phosphorous acid benzyl ester 2,3-bis-octyloxy-propyl ester methyl ester

There total 3 articles about Phosphorous acid benzyl ester 2,3-bis-octyloxy-propyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 111-83-1
1-bromo-octane

: 1028275-27-5
Phosphorous acid benzyl ester 2,3-bis-octyloxy-propyl ester methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / KOH / toluene / 24 h / Heating

2: 94 percent / H₂ / 10percent Pd/C / methanol / 2 h / 2585.7 Torr

3: 1.) N,N-diiisopropylethylamine / 1.) CH₂Cl₂, -78 deg C, 1 h, 2.) CH₂Cl₂, a) -78 deg C, 1 h, b) from -78 deg C to 25 deg C, 1 h

With potassium hydroxide; hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol; toluene;
DOI:10.1021/jm960434y

Reference yield:

: 140194-47-4
(+/-)-3-O-benzyl-1,2-di-O-octyl-sn-glycerol

: 1028275-27-5
Phosphorous acid benzyl ester 2,3-bis-octyloxy-propyl ester methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / H₂ / 10percent Pd/C / methanol / 2 h / 2585.7 Torr

2: 1.) N,N-diiisopropylethylamine / 1.) CH₂Cl₂, -78 deg C, 1 h, 2.) CH₂Cl₂, a) -78 deg C, 1 h, b) from -78 deg C to 25 deg C, 1 h

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol;
DOI:10.1021/jm960434y

Reference yield:

: 3279-26-3
methyl dichlorophosphite

: 22212-18-6
(+/-)-1,2-di-O-octyl-sn-glycerol

: 100-51-6,185532-71-2
benzyl alcohol

: 1028275-27-5
Phosphorous acid benzyl ester 2,3-bis-octyloxy-propyl ester methyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; Multistep reaction; 1.) CH₂Cl₂, -78 deg C, 1 h, 2.) CH₂Cl₂, a) -78 deg C, 1 h, b) from -78 deg C to 25 deg C, 1 h;
DOI:10.1021/jm960434y