cis-1,4-diacetoxy-1,4-bis(trimethylsilylethynyl)cyclohexa-2,5-diene

Base Information Edit

Chemical Name:cis-1,4-diacetoxy-1,4-bis(trimethylsilylethynyl)cyclohexa-2,5-diene
CAS No.:544706-67-4
Molecular Formula:C₂₀H₂₈O₄Si₂
Molecular Weight:388.611
Hs Code.:
Mol file:544706-67-4.mol

Synonyms:cis-1,4-diacetoxy-1,4-bis(trimethylsilylethynyl)cyclohexa-2,5-diene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-1,4-diacetoxy-1,4-bis(trimethylsilylethynyl)cyclohexa-2,5-diene Edit

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Technology Process of cis-1,4-diacetoxy-1,4-bis(trimethylsilylethynyl)cyclohexa-2,5-diene

There total 2 articles about cis-1,4-diacetoxy-1,4-bis(trimethylsilylethynyl)cyclohexa-2,5-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1066-54-2
trimethylsilylacetylene

: 544706-67-4
cis-1,4-diacetoxy-1,4-bis(trimethylsilylethynyl)cyclohexa-2,5-diene

Guidance literature:: Multi-step reaction with 2 steps

1.1: nBuLi / tetrahydrofuran / 0.75 h / -78 °C

1.2: tetrahydrofuran / 16 h / -78 - 10 °C

2.1: pyridine / 20 - 70 °C

With pyridine; n-butyllithium; In tetrahydrofuran;
DOI:10.1002/ejoc.200390106