(1S,2S)-N₁-(2,4-dimethoxyphenyl)-N₂-((S)-1-phenylethyl)cyclohexane-1,2-diamine

Base Information

Chemical Name:(1S,2S)-N₁-(2,4-dimethoxyphenyl)-N₂-((S)-1-phenylethyl)cyclohexane-1,2-diamine
CAS No.:1256796-15-2
Molecular Formula:C₂₂H₃₀N₂O₂
Molecular Weight:354.492
Hs Code.:

(1S,2S)-N<sub>1</sub>-(2,4-dimethoxyphenyl)-N<sub>2</sub>-((S)-1-phenylethyl)cyclohexane-1,2-diamine

Synonyms:(1S,2S)-N₁-(2,4-dimethoxyphenyl)-N₂-((S)-1-phenylethyl)cyclohexane-1,2-diamine

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Chemical Property of (1S,2S)-N₁-(2,4-dimethoxyphenyl)-N₂-((S)-1-phenylethyl)cyclohexane-1,2-diamine

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Technology Process of (1S,2S)-N₁-(2,4-dimethoxyphenyl)-N₂-((S)-1-phenylethyl)cyclohexane-1,2-diamine

There total 1 articles about (1S,2S)-N₁-(2,4-dimethoxyphenyl)-N₂-((S)-1-phenylethyl)cyclohexane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 212071-15-3
1-<(1S)-α-phenylethyl>-2,3-tetramethylene aziridine

: 2735-04-8,161687-55-4
2,4-Dimethoxyaniline

: 1256796-15-2
(1S,2S)-N₁-(2,4-dimethoxyphenyl)-N₂-((S)-1-phenylethyl)cyclohexane-1,2-diamine

: 1256796-18-5
(1R,2R)-N₁-(2,4-dimethoxyphenyl)-N₂-((S)-1-phenylethyl)cyclohexane-1,2-diamine

Guidance literature:: With tris(pentafluorophenyl)borate; In acetonitrile; at 65 ℃; for 36h; diastereoselective reaction; Inert atmosphere;
DOI:10.3390/molecules15118305

Reference yield:

: 1256796-15-2
(1S,2S)-N₁-(2,4-dimethoxyphenyl)-N₂-((S)-1-phenylethyl)cyclohexane-1,2-diamine

: C₁₄H₂₂N₂O₂

Guidance literature:: With 10% palladium on activated carbon; ammonium formate; In methanol; at 60 ℃; for 12h; Inert atmosphere;
DOI:10.3390/molecules15118305

Reference yield:

: 1256796-15-2
(1S,2S)-N₁-(2,4-dimethoxyphenyl)-N₂-((S)-1-phenylethyl)cyclohexane-1,2-diamine

: 1248337-30-5
1-(3,5-bis(trifluoromethyl)phenyl)-3-((1S,2S)-2-(2,4-dimethoxyphenylamino)cyclohexyl)thiourea

Guidance literature:: Multi-step reaction with 2 steps

1: 10% palladium on activated carbon; ammonium formate / methanol / 12 h / 60 °C / Inert atmosphere

2: dichloromethane / 3 h / 20 °C / Inert atmosphere

With 10% palladium on activated carbon; ammonium formate; In methanol; dichloromethane;
DOI:10.3390/molecules15118305