(2S,4S,5R)-2-Ethylsulfanyl-3,4-dimethyl-5-phenyl-[1,3,2]oxazaphospholidine 2-sulfide

Base Information

Chemical Name:(2S,4S,5R)-2-Ethylsulfanyl-3,4-dimethyl-5-phenyl-[1,3,2]oxazaphospholidine 2-sulfide
CAS No.:134355-88-7
Molecular Formula:C₁₂H₁₈NOPS₂
Molecular Weight:287.387
Hs Code.:

Synonyms:(2S,4S,5R)-2-Ethylsulfanyl-3,4-dimethyl-5-phenyl-[1,3,2]oxazaphospholidine 2-sulfide

Suppliers and Price of (2S,4S,5R)-2-Ethylsulfanyl-3,4-dimethyl-5-phenyl-[1,3,2]oxazaphospholidine 2-sulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4S,5R)-2-Ethylsulfanyl-3,4-dimethyl-5-phenyl-[1,3,2]oxazaphospholidine 2-sulfide

Chemical Property:

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Technology Process of (2S,4S,5R)-2-Ethylsulfanyl-3,4-dimethyl-5-phenyl-[1,3,2]oxazaphospholidine 2-sulfide

There total 1 articles about (2S,4S,5R)-2-Ethylsulfanyl-3,4-dimethyl-5-phenyl-[1,3,2]oxazaphospholidine 2-sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16001-05-1
dithiophosphorodichloridic acid ethyl ester

: 299-42-3,7009-81-6,90-83-5,6912-63-6
ephedrine

: 134355-88-7
(2S,4S,5R)-2-Ethylsulfanyl-3,4-dimethyl-5-phenyl-[1,3,2]oxazaphospholidine 2-sulfide

: 134273-29-3
(2R,4S,5R)-2-Ethylsulfanyl-3,4-dimethyl-5-phenyl-[1,3,2]oxazaphospholidine 2-sulfide

Guidance literature:: With triethylamine; In dichloromethane; at 5 ℃; for 18h;

Reference yield: 100.0%

: 134355-88-7
(2S,4S,5R)-2-Ethylsulfanyl-3,4-dimethyl-5-phenyl-[1,3,2]oxazaphospholidine 2-sulfide

: 134355-90-1
(R)-Dithiophosphoric acid O,S-diethyl ester O'-((1R,2S)-2-methylamino-1-phenyl-propyl) ester

Guidance literature:: With hydrogenchloride; In ethanol; at 25 ℃; for 1h;

Reference yield:

: 134355-88-7
(2S,4S,5R)-2-Ethylsulfanyl-3,4-dimethyl-5-phenyl-[1,3,2]oxazaphospholidine 2-sulfide

: 134273-33-9,134355-91-2
C₁₂H₂₀NO₃P

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / 4 N HCl / ethanol / 1 h / 25 °C

2: magnesium monoperoxyphthalate (MMPP) / H₂O / 20 h

With hydrogenchloride; magnesium monoperoxyphthalate hexahydrate; In ethanol; water;