(R)-Dithiophosphoric acid O,S-diethyl ester O'-((1R,2S)-2-methylamino-1-phenyl-propyl) ester

Base Information

Chemical Name:(R)-Dithiophosphoric acid O,S-diethyl ester O'-((1R,2S)-2-methylamino-1-phenyl-propyl) ester
CAS No.:134355-90-1
Molecular Formula:C₁₄H₂₄NO₂PS₂
Molecular Weight:333.456
Hs Code.:

Synonyms:(R)-Dithiophosphoric acid O,S-diethyl ester O'-((1R,2S)-2-methylamino-1-phenyl-propyl) ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-Dithiophosphoric acid O,S-diethyl ester O'-((1R,2S)-2-methylamino-1-phenyl-propyl) ester

Chemical Property:

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Technology Process of (R)-Dithiophosphoric acid O,S-diethyl ester O'-((1R,2S)-2-methylamino-1-phenyl-propyl) ester

There total 2 articles about (R)-Dithiophosphoric acid O,S-diethyl ester O'-((1R,2S)-2-methylamino-1-phenyl-propyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 134355-88-7
(2S,4S,5R)-2-Ethylsulfanyl-3,4-dimethyl-5-phenyl-[1,3,2]oxazaphospholidine 2-sulfide

: 134355-90-1
(R)-Dithiophosphoric acid O,S-diethyl ester O'-((1R,2S)-2-methylamino-1-phenyl-propyl) ester

Guidance literature:: With hydrogenchloride; In ethanol; at 25 ℃; for 1h;

Reference yield:

: 299-42-3,7009-81-6,90-83-5,6912-63-6
ephedrine

: 134355-90-1
(R)-Dithiophosphoric acid O,S-diethyl ester O'-((1R,2S)-2-methylamino-1-phenyl-propyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: NEt₃ / CH₂Cl₂ / 18 h / 5 °C

2: 100 percent / 4 N HCl / ethanol / 1 h / 25 °C

With hydrogenchloride; triethylamine; In ethanol; dichloromethane;

Reference yield:

: 134355-90-1
(R)-Dithiophosphoric acid O,S-diethyl ester O'-((1R,2S)-2-methylamino-1-phenyl-propyl) ester

: 134273-33-9,134355-91-2
C₁₂H₂₀NO₃P

: 134273-33-9,134355-91-2
C₁₂H₂₀NO₃P

Guidance literature:: With magnesium monoperoxyphthalate hexahydrate; In water; for 0.333333h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;