(6R,8S)-6,8-Dimethyl-5-trityloxymethyl-1,6,7,8-tetrahydro-cyclopenta[g]indole

Base Information

Chemical Name:(6R,8S)-6,8-Dimethyl-5-trityloxymethyl-1,6,7,8-tetrahydro-cyclopenta[g]indole
CAS No.:176979-93-4
Molecular Formula:C₃₃H₃₁NO
Molecular Weight:457.615
Hs Code.:

Synonyms:(6R,8S)-6,8-Dimethyl-5-trityloxymethyl-1,6,7,8-tetrahydro-cyclopenta[g]indole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (6R,8S)-6,8-Dimethyl-5-trityloxymethyl-1,6,7,8-tetrahydro-cyclopenta[g]indole

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Technology Process of (6R,8S)-6,8-Dimethyl-5-trityloxymethyl-1,6,7,8-tetrahydro-cyclopenta[g]indole

There total 4 articles about (6R,8S)-6,8-Dimethyl-5-trityloxymethyl-1,6,7,8-tetrahydro-cyclopenta[g]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 176979-92-3
Methanesulfonic acid (6R,8S)-8-methanesulfonyloxymethyl-5-trityloxymethyl-1,6,7,8-tetrahydro-cyclopenta[g]indol-6-ylmethyl ester

: 176979-93-4
(6R,8S)-6,8-Dimethyl-5-trityloxymethyl-1,6,7,8-tetrahydro-cyclopenta[g]indole

Guidance literature:: With sodium iodide; zinc; In 1,2-dimethoxyethane; for 5h; Heating; other reagent: lithium triethylborohydride;
DOI:10.1021/jo951767q

Reference yield:

: 176979-91-2
((6R,8S)-8-Hydroxymethyl-5-trityloxymethyl-1,6,7,8-tetrahydro-cyclopenta[g]indol-6-yl)-methanol

: 176979-93-4
(6R,8S)-6,8-Dimethyl-5-trityloxymethyl-1,6,7,8-tetrahydro-cyclopenta[g]indole

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / triethylamine / diethyl ether / 4 h / 0 °C

2: 69 percent / NaI, zinc / 1,2-dimethoxy-ethane / 5 h / Heating; other reagent: lithium triethylborohydride

With triethylamine; sodium iodide; zinc; In 1,2-dimethoxyethane; diethyl ether;
DOI:10.1021/jo951767q

Reference yield:

: 176980-00-0
(6R,8S)-1-(2,2-Dimethyl-propionyl)-5-trityloxymethyl-1,6,7,8-tetrahydro-cyclopenta[g]indole-6,8-dicarbaldehyde

: 176979-93-4
(6R,8S)-6,8-Dimethyl-5-trityloxymethyl-1,6,7,8-tetrahydro-cyclopenta[g]indole

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / sodium borohydride / methanol / 2 h / Ambient temperature

2: 83 percent / triethylamine / diethyl ether / 4 h / 0 °C

3: 69 percent / NaI, zinc / 1,2-dimethoxy-ethane / 5 h / Heating; other reagent: lithium triethylborohydride

With sodium tetrahydroborate; triethylamine; sodium iodide; zinc; In methanol; 1,2-dimethoxyethane; diethyl ether;
DOI:10.1021/jo951767q