6,6'-bis(3-tert-butyl-4-hydroxybenzyl)-4,4'-di-tert-butyl-2,2'-methanediyldiphenol

Base Information

Chemical Name:6,6'-bis(3-tert-butyl-4-hydroxybenzyl)-4,4'-di-tert-butyl-2,2'-methanediyldiphenol
CAS No.:1026706-99-9
Molecular Formula:C₄₃H₅₆O₄
Molecular Weight:636.915
Hs Code.:

Synonyms:6,6'-bis(3-tert-butyl-4-hydroxybenzyl)-4,4'-di-tert-butyl-2,2'-methanediyldiphenol

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Chemical Property of 6,6'-bis(3-tert-butyl-4-hydroxybenzyl)-4,4'-di-tert-butyl-2,2'-methanediyldiphenol

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Technology Process of 6,6'-bis(3-tert-butyl-4-hydroxybenzyl)-4,4'-di-tert-butyl-2,2'-methanediyldiphenol

There total 3 articles about 6,6'-bis(3-tert-butyl-4-hydroxybenzyl)-4,4'-di-tert-butyl-2,2'-methanediyldiphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 6,6'-bis(3-bromo-4-hydroxy-5-tert-butylbenzyl)-4,4'-di-tert-butyl-2,2'-methanediyldiphenol

: 1026706-99-9
6,6'-bis(3-tert-butyl-4-hydroxybenzyl)-4,4'-di-tert-butyl-2,2'-methanediyldiphenol

Guidance literature:: With potassium hydroxide; hydrogen; nickel; In methanol; at 20 ℃;
DOI:10.1021/jo970967u

Reference yield:

: 799-13-3
bis(5-tert-butyl-2-hydroxyphenyl)methane

: 1026706-99-9
6,6'-bis(3-tert-butyl-4-hydroxybenzyl)-4,4'-di-tert-butyl-2,2'-methanediyldiphenol

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / HBr / acetic acid / 5 h

2: 67 percent / ZnCO₃ / 16 h / 60 °C

3: 70 percent / KOH; hydrogen / Raney-nickel / methanol / 20 °C

With potassium hydroxide; hydrogen bromide; hydrogen; zinc(II) carbonate; nickel; In methanol; acetic acid; 1: Alkylation / 2: Alkylation / 3: Dehalogenation;
DOI:10.1021/jo970967u

Reference yield:

: 165318-85-4
6,6'-bis(bromomethyl)-4,4'-di-tert-butyl-2,2'-methanediyldiphenol

: 1026706-99-9
6,6'-bis(3-tert-butyl-4-hydroxybenzyl)-4,4'-di-tert-butyl-2,2'-methanediyldiphenol

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / ZnCO₃ / 16 h / 60 °C

2: 70 percent / KOH; hydrogen / Raney-nickel / methanol / 20 °C

With potassium hydroxide; hydrogen; zinc(II) carbonate; nickel; In methanol; 1: Alkylation / 2: Dehalogenation;
DOI:10.1021/jo970967u