C₁₆H₂₂O₃S

Base Information

Chemical Name:C₁₆H₂₂O₃S
CAS No.:1357179-56-6
Molecular Formula:C₁₆H₂₂O₃S
Molecular Weight:294.415
Hs Code.:

C<sub>16</sub>H<sub>22</sub>O<sub>3</sub>S

Synonyms:C₁₆H₂₂O₃S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₂₂O₃S

Chemical Property:

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Technology Process of C₁₆H₂₂O₃S

There total 5 articles about C₁₆H₂₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7697-61-2
2-cyclohexylacrylaldehyde

: 1357179-56-6
C₁₆H₂₂O₃S

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 2 h / 0 °C

2: triethylamine; trimethylamine hydrochloride / toluene / 0 - 25 °C

With sodium tetrahydroborate; trimethylamine hydrochloride; triethylamine; In methanol; toluene;
DOI:10.1002/anie.201304107

Reference yield:

: 1552-92-7
ethyl cyclohexylideneacetate

: 1357179-56-6
C₁₆H₂₂O₃S

Guidance literature:: Multi-step reaction with 5 steps

1: palladium on activated charcoal; hydrogen / ethanol / 5 h / 20 °C

2: diisobutylaluminium hydride / dichloromethane; hexane / 3 h / -78 °C

3: p-N,N-dimethylaminobenzoic acid; pyrrolidine / dichloromethane / Reflux; Inert atmosphere

4: sodium tetrahydroborate / methanol / 2 h / 0 °C

5: triethylamine; trimethylamine hydrochloride / toluene / 0 - 25 °C

With pyrrolidine; sodium tetrahydroborate; palladium on activated charcoal; hydrogen; p-N,N-dimethylaminobenzoic acid; trimethylamine hydrochloride; diisobutylaluminium hydride; triethylamine; In methanol; ethanol; hexane; dichloromethane; toluene;
DOI:10.1002/anie.201304107

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1357179-56-6
C₁₆H₂₂O₃S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 8 h / 20 °C

2.1: palladium on activated charcoal; hydrogen / ethanol / 5 h / 20 °C

3.1: diisobutylaluminium hydride / dichloromethane; hexane / 3 h / -78 °C

4.1: p-N,N-dimethylaminobenzoic acid; pyrrolidine / dichloromethane / Reflux; Inert atmosphere

5.1: sodium tetrahydroborate / methanol / 2 h / 0 °C

6.1: triethylamine; trimethylamine hydrochloride / toluene / 0 - 25 °C

With pyrrolidine; sodium tetrahydroborate; palladium on activated charcoal; hydrogen; p-N,N-dimethylaminobenzoic acid; trimethylamine hydrochloride; sodium hydride; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; toluene; mineral oil;
DOI:10.1002/anie.201304107