1-{1-[2-(tert-butyl-dimethylsilanyloxy)-1-methylethyl]-3-trimethylsilanylprop-2-ynyl}-2,3-dimethoxy-4-methyl benzene

Base Information

Chemical Name:1-{1-[2-(tert-butyl-dimethylsilanyloxy)-1-methylethyl]-3-trimethylsilanylprop-2-ynyl}-2,3-dimethoxy-4-methyl benzene
CAS No.:648433-56-1
Molecular Formula:C₂₄H₄₂O₃Si₂
Molecular Weight:434.767
Hs Code.:

Synonyms:1-{1-[2-(tert-butyl-dimethylsilanyloxy)-1-methylethyl]-3-trimethylsilanylprop-2-ynyl}-2,3-dimethoxy-4-methyl benzene

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Chemical Property of 1-{1-[2-(tert-butyl-dimethylsilanyloxy)-1-methylethyl]-3-trimethylsilanylprop-2-ynyl}-2,3-dimethoxy-4-methyl benzene

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Technology Process of 1-{1-[2-(tert-butyl-dimethylsilanyloxy)-1-methylethyl]-3-trimethylsilanylprop-2-ynyl}-2,3-dimethoxy-4-methyl benzene

There total 2 articles about 1-{1-[2-(tert-butyl-dimethylsilanyloxy)-1-methylethyl]-3-trimethylsilanylprop-2-ynyl}-2,3-dimethoxy-4-methyl benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6-(2,3-dimethoxy-4-methylphenyl)-5-methyl-8-trimethylsilanyl-oct-3-en-7-noic acid methyl ester

: 648433-56-1
1-{1-[2-(tert-butyl-dimethylsilanyloxy)-1-methylethyl]-3-trimethylsilanylprop-2-ynyl}-2,3-dimethoxy-4-methyl benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: Sudan III; O₃ / methanol / -78 °C

1.2: NaBH₄ / methanol / 3 h / -78 - 20 °C

2.1: 1.25 g / imidazole / dimethylformamide / 3 h

With 1H-imidazole; oil scarlet; ozone; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja039124c