2L-(2,3,5/4,6)-4,5-Di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycyclohexan

Base Information

Chemical Name:2L-(2,3,5/4,6)-4,5-Di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycyclohexan
CAS No.:81712-95-0
Molecular Formula:C₂₂H₂₆O₅
Molecular Weight:370.445
Hs Code.:

Synonyms:2L-(2,3,5/4,6)-4,5-Di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycyclohexan

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Chemical Property of 2L-(2,3,5/4,6)-4,5-Di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycyclohexan

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Technology Process of 2L-(2,3,5/4,6)-4,5-Di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycyclohexan

There total 4 articles about 2L-(2,3,5/4,6)-4,5-Di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycyclohexan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 81712-94-9
2L-(2,3,5/4,6)-4,5-Di-O-benzyl-2,3-O-isopropyliden-6-O-methyl-1-C-methylenpentahydroxycy

: 81712-95-0
2L-(2,3,5/4,6)-4,5-Di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycyclohexan

Guidance literature:: With acetic acid; In tetrahydrofuran; water; at 80 ℃; for 12h;
DOI:10.1016/S0008-6215(00)88052-0

Reference yield:

: 81712-93-8
1L-(1,2,4/3,5)-1,2-O-isopropylidene-5-O-methyl-6-methylenecyclohexane-1,2,3,4,5-pentol

: 81712-95-0
2L-(2,3,5/4,6)-4,5-Di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycyclohexan

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / sodium hydride / dimethylformamide

2: 97 percent / acetic acid / H₂O; tetrahydrofuran / 12 h / 80 °C

With sodium hydride; acetic acid; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)88052-0

Reference yield:

: 75251-60-4,75419-03-3
C₁₄H₂₂O₆

: 81712-95-0
2L-(2,3,5/4,6)-4,5-Di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycyclohexan

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / sodium diethyltellurophosphate / ethanol

2: 92 percent / 99 percent acetic acid / 72 h / Ambient temperature

3: 83 percent / sodium hydride / dimethylformamide

4: 97 percent / acetic acid / H₂O; tetrahydrofuran / 12 h / 80 °C

With sodium O,O-diethyl phosphorotelluroate; sodium hydride; acetic acid; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)88052-0