2L-(2,3,5/4,6)-3-O-Benzoyl-4,5-di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycy

Base Information

Chemical Name:2L-(2,3,5/4,6)-3-O-Benzoyl-4,5-di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycy
CAS No.:81712-96-1
Molecular Formula:C₂₉H₃₀O₆
Molecular Weight:474.554
Hs Code.:

Synonyms:2L-(2,3,5/4,6)-3-O-Benzoyl-4,5-di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycy

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Chemical Property of 2L-(2,3,5/4,6)-3-O-Benzoyl-4,5-di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycy

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Technology Process of 2L-(2,3,5/4,6)-3-O-Benzoyl-4,5-di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycy

There total 5 articles about 2L-(2,3,5/4,6)-3-O-Benzoyl-4,5-di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycy which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 98-88-4
benzoyl chloride

: 81712-95-0
2L-(2,3,5/4,6)-4,5-Di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycyclohexan

: 81712-96-1
2L-(2,3,5/4,6)-3-O-Benzoyl-4,5-di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycy

Guidance literature:: With pyridine; In chloroform; Ambient temperature;
DOI:10.1016/S0008-6215(00)88052-0

Reference yield:

: 81712-93-8
1L-(1,2,4/3,5)-1,2-O-isopropylidene-5-O-methyl-6-methylenecyclohexane-1,2,3,4,5-pentol

: 81712-96-1
2L-(2,3,5/4,6)-3-O-Benzoyl-4,5-di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycy

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / sodium hydride / dimethylformamide

2: 97 percent / acetic acid / H₂O; tetrahydrofuran / 12 h / 80 °C

3: 84 percent / pyridine / CHCl₃ / Ambient temperature

With pyridine; sodium hydride; acetic acid; In tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)88052-0

Reference yield:

: 81712-94-9
2L-(2,3,5/4,6)-4,5-Di-O-benzyl-2,3-O-isopropyliden-6-O-methyl-1-C-methylenpentahydroxycy

: 81712-96-1
2L-(2,3,5/4,6)-3-O-Benzoyl-4,5-di-O-benzyl-6-O-methyl-1-C-methylenpentahydroxycy

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / acetic acid / H₂O; tetrahydrofuran / 12 h / 80 °C

2: 84 percent / pyridine / CHCl₃ / Ambient temperature

With pyridine; acetic acid; In tetrahydrofuran; chloroform; water;
DOI:10.1016/S0008-6215(00)88052-0