C₄₀H₆₇IO₆Si

Base Information

Chemical Name:C₄₀H₆₇IO₆Si
CAS No.:1207069-57-5
Molecular Formula:C₄₀H₆₇IO₆Si
Molecular Weight:798.958
Hs Code.:

C<sub>40</sub>H<sub>67</sub>IO<sub>6</sub>Si

Synonyms:C₄₀H₆₇IO₆Si

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Chemical Property of C₄₀H₆₇IO₆Si

Chemical Property:

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Technology Process of C₄₀H₆₇IO₆Si

There total 13 articles about C₄₀H₆₇IO₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1207069-56-4
C₅₆H₈₅IO₆Si₂

: 1207069-57-5
C₄₀H₆₇IO₆Si

Guidance literature:: With potassium hydroxide; In methanol; at 60 ℃; for 20h;
DOI:10.1021/ol902778y

Reference yield:

: 910046-59-2
tert-butyl-[(3S)-(4-methoxybenzyloxy)hex-5-enyloxy]diphenylsilane

: 1207069-57-5
C₄₀H₆₇IO₆Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water / 20 °C

1.2: 20 °C

2.1: magnesium bromide diethyl etherate / dichloromethane / 0 °C

3.1: 2,6-dimethylpyridine / dichloromethane / 0 °C

4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 20 °C / pH 7 / aq. buffer

5.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 35 °C

6.1: potassium tert-butylate / tetrahydrofuran / 0 °C

7.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / -60 - -25 °C

8.1: 10% palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C

9.1: Dess-Martin periodane / dichloromethane / 20 °C

10.1: lithium hexamethyldisilazane / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 6 h / -78 - 20 °C

11.1: potassium hydroxide / tetrahydrofuran; methanol / 60 °C

With 2,6-dimethylpyridine; triethylsilane; osmium(VIII) oxide; Hoveyda-Grubbs catalyst second generation; magnesium bromide diethyl etherate; 10% palladium on activated charcoal; boron trifluoride diethyl etherate; potassium tert-butylate; hydrogen; Dess-Martin periodane; 4-methylmorpholine N-oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; ethyl acetate; 10.1: Julia Olefin synthesis;
DOI:10.1002/chem.201003135

Reference yield:

: C₄₁H₆₂O₄Si₂

: 1207069-57-5
C₄₀H₆₇IO₆Si

Guidance literature:: Multi-step reaction with 8 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 20 °C / pH 7 / aq. buffer

2: Hoveyda-Grubbs catalyst second generation / dichloromethane / 35 °C

3: potassium tert-butylate / tetrahydrofuran / 0 °C

4: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / -60 - -25 °C

5: 10% palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C

6: Dess-Martin periodane / dichloromethane / 20 °C

7: lithium hexamethyldisilazane / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 6 h / -78 - 20 °C

8: potassium hydroxide / tetrahydrofuran; methanol / 60 °C

With triethylsilane; Hoveyda-Grubbs catalyst second generation; 10% palladium on activated charcoal; boron trifluoride diethyl etherate; potassium tert-butylate; hydrogen; Dess-Martin periodane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; ethyl acetate; 7: Julia Olefin synthesis;
DOI:10.1002/chem.201003135