(2R,3S,4S,5S)-(+)-1-Benzyloxy-2,4-dimethoxy-8-(4'-methoxyphenoxy)-3,5-dimethyloctane

Base Information

Chemical Name:(2R,3S,4S,5S)-(+)-1-Benzyloxy-2,4-dimethoxy-8-(4'-methoxyphenoxy)-3,5-dimethyloctane
CAS No.:276690-12-1
Molecular Formula:C₂₆H₃₈O₅
Molecular Weight:430.585
Hs Code.:

Synonyms:(2R,3S,4S,5S)-(+)-1-Benzyloxy-2,4-dimethoxy-8-(4'-methoxyphenoxy)-3,5-dimethyloctane

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Chemical Property of (2R,3S,4S,5S)-(+)-1-Benzyloxy-2,4-dimethoxy-8-(4'-methoxyphenoxy)-3,5-dimethyloctane

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Technology Process of (2R,3S,4S,5S)-(+)-1-Benzyloxy-2,4-dimethoxy-8-(4'-methoxyphenoxy)-3,5-dimethyloctane

There total 1 articles about (2R,3S,4S,5S)-(+)-1-Benzyloxy-2,4-dimethoxy-8-(4'-methoxyphenoxy)-3,5-dimethyloctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 276690-16-5
(2R,3S,4S,5S)-(-)-1-Benzyloxy-8-(4'-methoxyphenoxy)-3,5-dimethyloctan-2,4-diol

: 74-88-4
methyl iodide

: 276690-12-1
(2R,3S,4S,5S)-(+)-1-Benzyloxy-2,4-dimethoxy-8-(4'-methoxyphenoxy)-3,5-dimethyloctane

Guidance literature:: With 18-crown-6 ether; potassium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 48h;

Reference yield: 90.0%

: 276690-12-1
(2R,3S,4S,5S)-(+)-1-Benzyloxy-2,4-dimethoxy-8-(4'-methoxyphenoxy)-3,5-dimethyloctane

: 276690-17-6
(4S,5S,6S,7R)-(+)-1-Benzyloxy-5,7-dimethoxy-4,6-dimethyloctan-1-ol

Guidance literature:: With ammonium cerium(IV) nitrate; water; In acetonitrile; at 0 ℃; for 0.1h;

Reference yield:

: 276690-12-1
(2R,3S,4S,5S)-(+)-1-Benzyloxy-2,4-dimethoxy-8-(4'-methoxyphenoxy)-3,5-dimethyloctane

: 276690-18-7
(4S,5S,6S,7R)-(+)-1-Benzyloxy-5,7-dimethoxy-4,6-dimethyloctanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / CAN; H₂O / acetonitrile / 0.1 h / 0 °C

2: 100 percent / PDC / dimethylformamide / 20 °C

With dipyridinium dichromate; ammonium cerium(IV) nitrate; water; In N,N-dimethyl-formamide; acetonitrile; 1: Oxidation / 2: Oxidation;