3-{[6-(3-chlorophenyl)-4-({2-[(1-methylethyl)amino]-2-oxoethyl}oxy)pyrazolo[1,5-a]pyrazin-2-yl]oxy}propyl acetate

Base Information

Chemical Name:3-{[6-(3-chlorophenyl)-4-({2-[(1-methylethyl)amino]-2-oxoethyl}oxy)pyrazolo[1,5-a]pyrazin-2-yl]oxy}propyl acetate
CAS No.:1192313-25-9
Molecular Formula:C₂₂H₂₅ClN₄O₅
Molecular Weight:460.917
Hs Code.:

Synonyms:3-{[6-(3-chlorophenyl)-4-({2-[(1-methylethyl)amino]-2-oxoethyl}oxy)pyrazolo[1,5-a]pyrazin-2-yl]oxy}propyl acetate

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Chemical Property of 3-{[6-(3-chlorophenyl)-4-({2-[(1-methylethyl)amino]-2-oxoethyl}oxy)pyrazolo[1,5-a]pyrazin-2-yl]oxy}propyl acetate

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Technology Process of 3-{[6-(3-chlorophenyl)-4-({2-[(1-methylethyl)amino]-2-oxoethyl}oxy)pyrazolo[1,5-a]pyrazin-2-yl]oxy}propyl acetate

There total 4 articles about 3-{[6-(3-chlorophenyl)-4-({2-[(1-methylethyl)amino]-2-oxoethyl}oxy)pyrazolo[1,5-a]pyrazin-2-yl]oxy}propyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2895-21-8
2-chloro-N-isopropylacetamide

: 1192313-23-7
3-{[6-(3-chlorophenyl)-4-oxo-4,5-dihydropyrazolo[1,5-a]pyrazin-2-yl]oxy}propyl acetate

: 1192313-24-8
3-[(6-(3-chlorophenyl)-5-{2-[(1-methylethyl)amino]-2-oxoethyl}-4-oxo-4,5-dihydropyrazolo[1,5-a]pyrazin-2-yl)oxy]propyl acetate

: 1192313-25-9
3-{[6-(3-chlorophenyl)-4-({2-[(1-methylethyl)amino]-2-oxoethyl}oxy)pyrazolo[1,5-a]pyrazin-2-yl]oxy}propyl acetate

Guidance literature:: 3-{[6-(3-chlorophenyl)-4-oxo-4,5-dihydropyrazolo[1,5-a]pyrazin-2-yl]oxy}propyl acetate; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃;

2-chloro-N-isopropylacetamide; With sodium iodide; In N,N-dimethyl-formamide; at 0 - 70 ℃;

Reference yield:

: 1192313-21-5
ethyl 3-[(3-{[(1,1-dimethylethyl)(dimethyl)silyl]oxy}propyl)oxy]-1H-pyrazole-5-carboxylate

: 1192313-24-8
3-[(6-(3-chlorophenyl)-5-{2-[(1-methylethyl)amino]-2-oxoethyl}-4-oxo-4,5-dihydropyrazolo[1,5-a]pyrazin-2-yl)oxy]propyl acetate

: 1192313-25-9
3-{[6-(3-chlorophenyl)-4-({2-[(1-methylethyl)amino]-2-oxoethyl}oxy)pyrazolo[1,5-a]pyrazin-2-yl]oxy}propyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate / N,N-dimethyl-formamide / 20 - 60 °C

2.1: 24 h / 100 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

3.2: 0 - 70 °C

With sodium hydride; sodium carbonate; In N,N-dimethyl-formamide;

Reference yield:

: 1192313-22-6
ethyl 1-[2-(3-chlorophenyl)-2-oxoethyl]-3-[(3-{[(1,1-dimethylethyl)(dimethyl)silyl]oxy}propyl)oxy]-1H-pyrazole-5-carboxylate

: 1192313-24-8
3-[(6-(3-chlorophenyl)-5-{2-[(1-methylethyl)amino]-2-oxoethyl}-4-oxo-4,5-dihydropyrazolo[1,5-a]pyrazin-2-yl)oxy]propyl acetate

: 1192313-25-9
3-{[6-(3-chlorophenyl)-4-({2-[(1-methylethyl)amino]-2-oxoethyl}oxy)pyrazolo[1,5-a]pyrazin-2-yl]oxy}propyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 24 h / 100 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

2.2: 0 - 70 °C

With sodium hydride; In N,N-dimethyl-formamide;