benzyl 1-deoxy-4,5-O-isopropylidene-D-erythro-2,3-hexodiulo-3,6-furanoside

Base Information

Chemical Name:benzyl 1-deoxy-4,5-O-isopropylidene-D-erythro-2,3-hexodiulo-3,6-furanoside
CAS No.:86782-07-2
Molecular Formula:C₁₆H₂₀O₅
Molecular Weight:292.332
Hs Code.:

Synonyms:benzyl 1-deoxy-4,5-O-isopropylidene-D-erythro-2,3-hexodiulo-3,6-furanoside

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Chemical Property of benzyl 1-deoxy-4,5-O-isopropylidene-D-erythro-2,3-hexodiulo-3,6-furanoside

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Technology Process of benzyl 1-deoxy-4,5-O-isopropylidene-D-erythro-2,3-hexodiulo-3,6-furanoside

There total 3 articles about benzyl 1-deoxy-4,5-O-isopropylidene-D-erythro-2,3-hexodiulo-3,6-furanoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 86782-06-1
3,6-anhydro-4,5-O-isopropylidene-1-O-tosyl-D-fructose

: 100-51-6,185532-71-2
benzyl alcohol

: 86782-07-2
benzyl 1-deoxy-4,5-O-isopropylidene-D-erythro-2,3-hexodiulo-3,6-furanoside

Guidance literature:: With toluene-4-sulfonic acid; triethylamine; at 70 ℃; for 30h; Heating;
DOI:10.1016/0008-6215(83)88110-5

Reference yield:

: 53577-84-7,53776-55-9
3,6-anhydro-4,5-O-isopropylidene-1-O-tosyl-D-mannitol

: 86782-07-2
benzyl 1-deoxy-4,5-O-isopropylidene-D-erythro-2,3-hexodiulo-3,6-furanoside

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / ruthenium dioxide, potassium periodate, potassium carbonate / CHCl₃; H₂O / 19 h

2: 79 percent / triethylamine, p-toluenesulfonic acid / 30 h / 70 °C / Heating

With ruthenium(IV) oxide; potassium metaperiodate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; In chloroform; water;
DOI:10.1016/0008-6215(83)88110-5

Reference yield:

: 2270-08-8,53626-11-2,71485-96-6
3,6-anhydro-4,5-O-isopropylidene-D-mannitol

: 86782-07-2
benzyl 1-deoxy-4,5-O-isopropylidene-D-erythro-2,3-hexodiulo-3,6-furanoside

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / pyridine; CH₂Cl₂ / 1.) 0 deg C, 2 h; 2.) r.t., 18 h

2: 65 percent / ruthenium dioxide, potassium periodate, potassium carbonate / CHCl₃; H₂O / 19 h

3: 79 percent / triethylamine, p-toluenesulfonic acid / 30 h / 70 °C / Heating

With ruthenium(IV) oxide; potassium metaperiodate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; In pyridine; dichloromethane; chloroform; water;
DOI:10.1016/0008-6215(83)88110-5