11-tert-butyl 5-(2-isopropyl-5-methylcyclohexyl) 2-bromo-7,8,9,10-tetrahydro-7,10-epiminocyclohepta[b]indole-5,11(6H)-dicarboxylate

Base Information

Chemical Name:11-tert-butyl 5-(2-isopropyl-5-methylcyclohexyl) 2-bromo-7,8,9,10-tetrahydro-7,10-epiminocyclohepta[b]indole-5,11(6H)-dicarboxylate
CAS No.:1416007-23-2
Molecular Formula:C₂₉H₃₉BrN₂O₄
Molecular Weight:559.544
Hs Code.:

Synonyms:11-tert-butyl 5-(2-isopropyl-5-methylcyclohexyl) 2-bromo-7,8,9,10-tetrahydro-7,10-epiminocyclohepta[b]indole-5,11(6H)-dicarboxylate

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Chemical Property of 11-tert-butyl 5-(2-isopropyl-5-methylcyclohexyl) 2-bromo-7,8,9,10-tetrahydro-7,10-epiminocyclohepta[b]indole-5,11(6H)-dicarboxylate

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Technology Process of 11-tert-butyl 5-(2-isopropyl-5-methylcyclohexyl) 2-bromo-7,8,9,10-tetrahydro-7,10-epiminocyclohepta[b]indole-5,11(6H)-dicarboxylate

There total 4 articles about 11-tert-butyl 5-(2-isopropyl-5-methylcyclohexyl) 2-bromo-7,8,9,10-tetrahydro-7,10-epiminocyclohepta[b]indole-5,11(6H)-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-butyl 2-bromo-5,6,7,8,9,10-hexahydro-7,10-epiminocyclohepta[b]indole-11-carboxylate

: 7635-54-3,7635-53-2
(+)-(1S,2R,5S)-menthylchloroformate

: 1416007-23-2
11-tert-butyl 5-(2-isopropyl-5-methylcyclohexyl) 2-bromo-7,8,9,10-tetrahydro-7,10-epiminocyclohepta[b]indole-5,11(6H)-dicarboxylate

Guidance literature:: With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In dichloromethane; water; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.tetasy.2012.10.012

Reference yield:

: 622-88-8,41931-18-4
4-bromophenylhydrazine hydrochloride

: 1416007-23-2
11-tert-butyl 5-(2-isopropyl-5-methylcyclohexyl) 2-bromo-7,8,9,10-tetrahydro-7,10-epiminocyclohepta[b]indole-5,11(6H)-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol / 4 h / Inert atmosphere; Reflux

1.2: 65 h / Inert atmosphere; Reflux

2.1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / water; dichloromethane / 4 h / 20 °C / Inert atmosphere

With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In ethanol; dichloromethane; water; 1.1: |Fischer Indole Synthesis / 1.2: |Fischer Indole Synthesis;
DOI:10.1016/j.tetasy.2012.10.012

Reference yield:

: 25602-68-0
3-oxo-8-azabicyclo[3.2.1]octane hydrochloride

: 1416007-23-2
11-tert-butyl 5-(2-isopropyl-5-methylcyclohexyl) 2-bromo-7,8,9,10-tetrahydro-7,10-epiminocyclohepta[b]indole-5,11(6H)-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol / 4 h / Inert atmosphere; Reflux

1.2: 65 h / Inert atmosphere; Reflux

2.1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / water; dichloromethane / 4 h / 20 °C / Inert atmosphere

With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In ethanol; dichloromethane; water; 1.1: |Fischer Indole Synthesis / 1.2: |Fischer Indole Synthesis;
DOI:10.1016/j.tetasy.2012.10.012