2,2,5,5-tetramethyl-1-cyclopentane

Base Information

Chemical Name:2,2,5,5-tetramethyl-1-cyclopentane
CAS No.:138235-27-5
Molecular Formula:C₂₄H₃₆N₂S
Molecular Weight:384.629
Hs Code.:

2,2,5,5-tetramethyl-1-<N-(2',4'-di-tert-butyl-6'-cyanophenyl)sulfinimidoyl>cyclopentane

Synonyms:2,2,5,5-tetramethyl-1-cyclopentane

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Chemical Property of 2,2,5,5-tetramethyl-1-cyclopentane

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Technology Process of 2,2,5,5-tetramethyl-1-cyclopentane

There total 3 articles about 2,2,5,5-tetramethyl-1-cyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 127204-57-3
7-azido-2,4-di-tert-butyl-8,9-thiazabicyclo<4.3.0>nona-2,4,6,9-tetraene

: 71690-98-7
2-Diazo-1,1,3,3-tetramethylcyclopentane

: 17582-88-6
2,4-di-tert-butyl-6-cyanoaniline

: 138235-27-5
2,2,5,5-tetramethyl-1-cyclopentane

: 127204-58-4
N,N'-bis(2,4-di-tert-butyl-6-cyanophenyl)sulfur diimide

: 127616-57-3
N-(2,4-di-tert-butyl-6-cyanophenyl)-N'-(2',4'-di-tert-butyl-8',9'-thiazabicyclo<4.3.0>nona-2',4',6',9'-tetraen-7'-yl)sulfur diimide

Guidance literature:: In hexane; at 30 ℃; for 48h;
DOI:10.1021/ja00031a043

Reference yield:

: 63335-28-4
2,4-di-tert-butyl-8,9-thiazabicyclo<4.3.0>nona-2,4,6,9-tetraene

: 138235-27-5
2,2,5,5-tetramethyl-1-cyclopentane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi, 2.) (trimethylsilyl)methyl azide, 3.) H₂O

3: 54 percent / hexane / 48 h / 30 °C

With n-butyllithium; water; trimethylsilylmethyl azide; In hexane;
DOI:10.1021/ja00031a043