2-allyl-2-trifluoromethylpent-4-enoic acid

Base Information

Chemical Name:2-allyl-2-trifluoromethylpent-4-enoic acid
CAS No.:1115036-27-5
Molecular Formula:C₉H₁₁F₃O₂
Molecular Weight:208.18
Hs Code.:

Synonyms:2-allyl-2-trifluoromethylpent-4-enoic acid

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Chemical Property of 2-allyl-2-trifluoromethylpent-4-enoic acid

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Technology Process of 2-allyl-2-trifluoromethylpent-4-enoic acid

There total 1 articles about 2-allyl-2-trifluoromethylpent-4-enoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 912334-55-5
benzyl 2,2-diallyl-3,3,3-trifluorodithiopropanoate

: 150-60-7
dibenzyl disulphide

: 1115036-27-5
2-allyl-2-trifluoromethylpent-4-enoic acid

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; In methanol; water; at 20 ℃; for 0.0833333h;
DOI:10.1055/s-0028-1083190

Reference yield:

: 1115036-27-5
2-allyl-2-trifluoromethylpent-4-enoic acid

: 3-benzylamino-1-(trifluoromethyl)cyclopentane-1-carboxylic acid hydrochloride

Guidance literature:: Multi-step reaction with 7 steps

1.1: Grubbs catalyst first generation / dichloromethane / 2 h / 20 °C / Inert atmosphere

2.1: oxygen; palladium diacetate / water; acetonitrile / 16 h / 50 °C

3.1: caesium carbonate / acetone

4.1: acetic acid / tetrahydrofuran / 0.67 h / 20 °C / Inert atmosphere

4.2: 2.75 h / 20 °C / Inert atmosphere

5.1: water; sodium hydroxide / ethanol / 15 h / 0 - 20 °C

6.1: thionyl chloride / 15 h / 50 °C

7.1: potassium tert-butylate / water; dimethyl sulfoxide / 18 h / 100 °C

7.2: 20 °C

With Grubbs catalyst first generation; thionyl chloride; potassium tert-butylate; water; oxygen; palladium diacetate; caesium carbonate; acetic acid; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide; acetone; acetonitrile; 2.1: Wacker oxidation;
DOI:10.1002/ejoc.201101321

Reference yield:

: 1115036-27-5
2-allyl-2-trifluoromethylpent-4-enoic acid

: benzyl c-3,c-4-epoxy-1-(trifluoromethyl)cyclopentane-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: Grubbs catalyst first generation / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: iodine; sodium hydrogencarbonate; potassium iodide / tetrahydrofuran; water / 72 h / 20 °C

3: benzyl alcohol / 0 - 20 °C / Inert atmosphere

With Grubbs catalyst first generation; iodine; sodium hydrogencarbonate; potassium iodide; In tetrahydrofuran; dichloromethane; water; benzyl alcohol;
DOI:10.1002/ejoc.201101321