Technology Process of C50H31N5Pd
There total 5 articles about C50H31N5Pd which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis(acetylacetonato)palladium(II);
In
toluene;
for 40h;
Inert atmosphere;
Reflux;
DOI:10.1142/S108842461100346X
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium tert-butylate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 100 °C / Inert atmosphere
2: nitrobenzene / 19 h / Reflux
3: sulfuric acid; trifluoroacetic acid / 0.75 h
4: bis(acetylacetonato)palladium(II) / toluene / 40 h / Inert atmosphere; Reflux
With
bis(acetylacetonato)palladium(II); sulfuric acid; potassium tert-butylate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; trifluoroacetic acid;
In
nitrobenzene; toluene;
1: Buchwald-Hartwig amination;
DOI:10.1142/S108842461100346X
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogenchloride; tin / chloroform; water / 20 °C
2: potassium tert-butylate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 100 °C / Inert atmosphere
3: nitrobenzene / 19 h / Reflux
4: sulfuric acid; trifluoroacetic acid / 0.75 h
5: bis(acetylacetonato)palladium(II) / toluene / 40 h / Inert atmosphere; Reflux
With
hydrogenchloride; tin; bis(acetylacetonato)palladium(II); sulfuric acid; potassium tert-butylate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; trifluoroacetic acid;
In
chloroform; water; nitrobenzene; toluene;
2: Buchwald-Hartwig amination;
DOI:10.1142/S108842461100346X
