1-(4-(5-amino-3-tert-butyl-1H-pyrazol-1-yl)phenyl)-N-methyl methanesulfonamide

Base Information

Chemical Name:1-(4-(5-amino-3-tert-butyl-1H-pyrazol-1-yl)phenyl)-N-methyl methanesulfonamide
CAS No.:1338815-24-9
Molecular Formula:C₁₅H₂₂N₄O₂S
Molecular Weight:322.431
Hs Code.:

Synonyms:1-(4-(5-amino-3-tert-butyl-1H-pyrazol-1-yl)phenyl)-N-methyl methanesulfonamide

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Chemical Property of 1-(4-(5-amino-3-tert-butyl-1H-pyrazol-1-yl)phenyl)-N-methyl methanesulfonamide

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Technology Process of 1-(4-(5-amino-3-tert-butyl-1H-pyrazol-1-yl)phenyl)-N-methyl methanesulfonamide

There total 2 articles about 1-(4-(5-amino-3-tert-butyl-1H-pyrazol-1-yl)phenyl)-N-methyl methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59997-51-2
trimethylacetylacetonitrile

: 139272-29-0
4-hydrazinobenzyl methyl sulfone

: 1338815-24-9
1-(4-(5-amino-3-tert-butyl-1H-pyrazol-1-yl)phenyl)-N-methyl methanesulfonamide

Guidance literature:: trimethylacetylacetonitrile; 4-hydrazinobenzyl methyl sulfone; With hydrogenchloride; In ethanol; water; at 20 ℃; for 28h; Reflux;

With sodium hydroxide; In water;

Reference yield:

: 109903-35-7
1-(4-aminophenyl)-N-methylmethanesulfonamide

: 1338815-24-9
1-(4-(5-amino-3-tert-butyl-1H-pyrazol-1-yl)phenyl)-N-methyl methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / water / 2.58 h / 0 °C

1.2: 64 h / 0 - 20 °C

1.3: pH 12

2.1: hydrogenchloride / ethanol; water / 28 h / 20 °C / Reflux

With hydrogenchloride; sodium nitrite; In ethanol; water;