Pd(C₆H₅)(NH(CH₂CH₂P(CH(CH₃)2)2)2)⁽¹⁺⁾*PF₆^(1-)=(Pd(C₆H₅)(NH(CH₂CH₂P(CH(CH₃)2)2)2))PF₆

Base Information

• Chemical Name: Pd(C₆H₅)(NH(CH₂CH₂P(CH(CH₃)2)2)2)⁽¹⁺⁾*PF₆^(1-)=(Pd(C₆H₅)(NH(CH₂CH₂P(CH(CH₃)2)2)2))PF₆
• CAS No.: 1140920-85-9
• Molecular Formula: C₂₂H₄₂NP₂Pd*F₆P
• Molecular Weight: 633.914

Synonyms:Pd(C₆H₅)(NH(CH₂CH₂P(CH(CH₃)2)2)2)⁽¹⁺⁾*PF₆^(1-)=(Pd(C₆H₅)(NH(CH₂CH₂P(CH(CH₃)2)2)2))PF₆

Chemical Property of Pd(C₆H₅)(NH(CH₂CH₂P(CH(CH₃)2)2)2)⁽¹⁺⁾*PF₆^(1-)=(Pd(C₆H₅)(NH(CH₂CH₂P(CH(CH₃)2)2)2))PF₆

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Technology Process of Pd(C₆H₅)(NH(CH₂CH₂P(CH(CH₃)2)2)2)⁽¹⁺⁾*PF₆^(1-)=(Pd(C₆H₅)(NH(CH₂CH₂P(CH(CH₃)2)2)2))PF₆

There total 3 articles about Pd(C₆H₅)(NH(CH₂CH₂P(CH(CH₃)2)2)2)⁽¹⁺⁾*PF₆^(1-)=(Pd(C₆H₅)(NH(CH₂CH₂P(CH(CH₃)2)2)2))PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

bis[2-(di-iso-propylphosphino)ethyl]amine (131890-26-1) + silver(I) hexafluorophosphate (26042-63-7) + (N,N,N',N'-tetramethylethylenediamine)Pd(phenyl)I → Pd(C6H5)(NH(CH2CH2P(CH(CH3)2)2)2)(1+)*PF6(1-)=(Pd(C6H5)(NH(CH2CH2P(CH(CH3)2)2)2))PF6 (1140920-85-9)

Guidance literature:

In tetrahydrofuran; under Ar; soln. of ligand in THF added dropwise to soln. of Pd complex in THF; stirred at room temp. for 30 min; filtered; ppt. washed with Et2O; dried in vac.; dissolved in CH2Cl2; soln. of AgPF6 in CH2Cl2 added dropwise; stirred for 15 min; filtered; ppt. washed with Et2O; pptd. from filtrate with Et2O and pentanes; washed with Et2O; dried in vac.; elem. anal.;

DOI:10.1021/ic802286u

Reference yield:

silver(I) hexafluorophosphate (26042-63-7) + Pd(C6H5)(N(CH2CH2P(CH(CH3)2)2)2) (1140920-88-2) → Pd(C6H5)(N(CH2CH2P(CH(CH3)2)2)CHCH2P(CH(CH3)2)2)(1+)*PF6(1-)=(Pd(C6H5)(N(CH2CH2P(CH(CH3)2)2)CHCH2P(CH(CH3)2)2))PF6 (1140920-94-0) + Pd(C6H5)(NH(CH2CH2P(CH(CH3)2)2)2)(1+)*PF6(1-)=(Pd(C6H5)(NH(CH2CH2P(CH(CH3)2)2)2))PF6 (1140920-85-9)

Guidance literature:

In tetrahydrofuran; under Ar; in NMR tube; AgPF6 added at room temp. to soln. of Pd complex in THF; 5 min; not isolated; detd. by (1)H and (31)P NMR spectra;

DOI:10.1021/ic802286u

Reference yield:

tetrahydrofuran-d8 (1693-74-9) + silver(I) hexafluorophosphate (26042-63-7) + Pd(C6H5)(N(CH2CH2P(CH(CH3)2)2)2) (1140920-88-2) → Pd(C6H5)(N(CH2CH2P(CH(CH3)2)2)CHCH2P(CH(CH3)2)2)(1+)*PF6(1-)=(Pd(C6H5)(N(CH2CH2P(CH(CH3)2)2)CHCH2P(CH(CH3)2)2))PF6 (1140920-94-0) + Pd(C6H5)(NH(CH2CH2P(CH(CH3)2)2)2)(1+)*PF6(1-)=(Pd(C6H5)(NH(CH2CH2P(CH(CH3)2)2)2))PF6 (1140920-85-9) + Pd(C6H5)(N(2)H(CH2CH2P(CH(CH3)2)2)2)(1+)*PF6(1-)=(Pd(C6H5)(N(2)H(CH2CH2P(CH(CH3)2)2)2))PF6

Guidance literature:

In tetrahydrofuran-d8; under Ar; in NMR tube; AgPF6 added at room temp. to soln. of Pd complex in THF-d8; 5 min; not isolated; detd. by (2)H and (31)P NMR spectra;

DOI:10.1021/ic802286u

upstream raw materials:

bis[2-(di-iso-propylphosphino)ethyl]amine

silver(I) hexafluorophosphate

Pd(C₆H₅)(N(CH₂CH₂P(CH(CH₃)2)2)2)

tetrahydrofuran-d8

Downstream raw materials:

Pd(C₆H₅)(N(CH₂CH₂P(CH(CH₃)2)2)2)

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