6-(2-chloro-4-methoxy-phenyl)-N₄-(1-propyl-butyl)-pyrimidine-4,5-diamine

Base Information

Chemical Name:6-(2-chloro-4-methoxy-phenyl)-N₄-(1-propyl-butyl)-pyrimidine-4,5-diamine
CAS No.:677743-93-0
Molecular Formula:C₁₈H₂₅ClN₄O
Molecular Weight:348.876
Hs Code.:

6-(2-chloro-4-methoxy-phenyl)-N<sub>4</sub>-(1-propyl-butyl)-pyrimidine-4,5-diamine

Synonyms:6-(2-chloro-4-methoxy-phenyl)-N₄-(1-propyl-butyl)-pyrimidine-4,5-diamine

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Chemical Property of 6-(2-chloro-4-methoxy-phenyl)-N₄-(1-propyl-butyl)-pyrimidine-4,5-diamine

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Technology Process of 6-(2-chloro-4-methoxy-phenyl)-N₄-(1-propyl-butyl)-pyrimidine-4,5-diamine

There total 2 articles about 6-(2-chloro-4-methoxy-phenyl)-N₄-(1-propyl-butyl)-pyrimidine-4,5-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 4316-93-2
4,6-dichloro-5-nitropyrimidine

: 219735-99-6
2-chloro-4-methoxyphenylboronic acid

: 677743-93-0
6-(2-chloro-4-methoxy-phenyl)-N₄-(1-propyl-butyl)-pyrimidine-4,5-diamine

Guidance literature:: 4,6-dichloro-5-nitropyrimidine; 2-chloro-4-methoxyphenylboronic acid; With sodium carbonate; bis-triphenylphosphine-palladium(II) chloride; In ethanol; toluene; for 5h; Heating / reflux;

With 4-heptylamine; In butan-1-ol; for 18h; Heating / reflux;

Reference yield:

: (R)-6-(2-chloro-4-methoxy-phenyl)-N₄-(1-cyclopropyl-ethyl)-pyrimidine-4,5-diamine

: 677743-93-0
6-(2-chloro-4-methoxy-phenyl)-N₄-(1-propyl-butyl)-pyrimidine-4,5-diamine

Guidance literature:: (R)-6-(2-chloro-4-methoxy-phenyl)-N₄-(1-cyclopropyl-ethyl)-pyrimidine-4,5-diamine; With 2-oxo-propionic acid ethyl ester; In ethanol; for 18h;

In acetic acid; at 100 ℃; for 1h;

Reference yield:

: 677743-93-0
6-(2-chloro-4-methoxy-phenyl)-N₄-(1-propyl-butyl)-pyrimidine-4,5-diamine

: 677743-92-9
4-(2-CHLORO-4-METHOXY-PHENYL)-6-METHYL-8-(L-PROPYL-BUTYL)-8H-PTERIDIN-7-ONE

Guidance literature:: 6-(2-chloro-4-methoxy-phenyl)-N₄-(1-propyl-butyl)-pyrimidine-4,5-diamine; With 2-oxo-propionic acid ethyl ester; In ethanol; for 18h;

In acetic acid; at 100 ℃; for 1h;