N,N-diethyl-5,6-dihydro-5-p-methoxybenzyl-6-oxo-phenanthridine-2-carboxamide

Base Information

Chemical Name:N,N-diethyl-5,6-dihydro-5-p-methoxybenzyl-6-oxo-phenanthridine-2-carboxamide
CAS No.:1616679-87-8
Molecular Formula:C₂₆H₂₆N₂O₃
Molecular Weight:414.504
Hs Code.:

Synonyms:N,N-diethyl-5,6-dihydro-5-p-methoxybenzyl-6-oxo-phenanthridine-2-carboxamide

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Chemical Property of N,N-diethyl-5,6-dihydro-5-p-methoxybenzyl-6-oxo-phenanthridine-2-carboxamide

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Technology Process of N,N-diethyl-5,6-dihydro-5-p-methoxybenzyl-6-oxo-phenanthridine-2-carboxamide

There total 4 articles about N,N-diethyl-5,6-dihydro-5-p-methoxybenzyl-6-oxo-phenanthridine-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1616680-79-5
N,N-diethyl-4-[(2-bromobenzoyl)-p-methoxybenzyl]aminobenzoic amide

: 1616679-87-8
N,N-diethyl-5,6-dihydro-5-p-methoxybenzyl-6-oxo-phenanthridine-2-carboxamide

Guidance literature:: With palladium diacetate; caesium carbonate; tricyclohexylphosphine tetrafluoroborate; In N,N-dimethyl acetamide; at 130 ℃; for 4h;
DOI:10.1016/j.bmc.2014.05.022

Reference yield:

: 51207-85-3
4-amino-N,N-diethylbenzamide

: 1616679-87-8
N,N-diethyl-5,6-dihydro-5-p-methoxybenzyl-6-oxo-phenanthridine-2-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / dichloromethane; water / 15 h / 0 - 20 °C

2: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

3: palladium diacetate; caesium carbonate; tricyclohexylphosphine tetrafluoroborate / N,N-dimethyl acetamide / 4 h / 130 °C

With palladium diacetate; sodium hydride; sodium hydrogencarbonate; caesium carbonate; tricyclohexylphosphine tetrafluoroborate; In dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; 3: |Heck Reaction;
DOI:10.1016/j.bmc.2014.05.022

Reference yield:

: 903255-01-6
N,N-diethyl-4-(2-bromobenzoyl)aminobenzoic amide

: 1616679-87-8
N,N-diethyl-5,6-dihydro-5-p-methoxybenzyl-6-oxo-phenanthridine-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

2: palladium diacetate; caesium carbonate; tricyclohexylphosphine tetrafluoroborate / N,N-dimethyl acetamide / 4 h / 130 °C

With palladium diacetate; sodium hydride; caesium carbonate; tricyclohexylphosphine tetrafluoroborate; In N,N-dimethyl acetamide; N,N-dimethyl-formamide; 2: |Heck Reaction;
DOI:10.1016/j.bmc.2014.05.022