Technology Process of C24H25Cl2F2N3O6S
There total 7 articles about C24H25Cl2F2N3O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap; dicyclohexyl-carbodiimide;
In
dichloromethane;
at 15 ℃;
for 2.5h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium carbonate / acetonitrile / 4 h / Inert atmosphere; Reflux
2.1: sodium chlorite; aminosulfonic acid; acetic acid / water / 0.5 h / 5 - 10 °C
3.1: thionyl chloride / toluene / 1.5 h / 90 °C / Inert atmosphere
4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 10 °C / Inert atmosphere
5.1: lithium hydroxide / methanol / 1.33 h / 60 °C
5.2: pH 4
6.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 2.5 h / 15 °C / Inert atmosphere
With
dmap; sodium chlorite; thionyl chloride; aminosulfonic acid; sodium hydride; potassium carbonate; acetic acid; dicyclohexyl-carbodiimide; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; toluene; acetonitrile; mineral oil;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 10 °C / Inert atmosphere
2.1: lithium hydroxide / methanol / 1.33 h / 60 °C
2.2: pH 4
3.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 2.5 h / 15 °C / Inert atmosphere
With
dmap; sodium hydride; dicyclohexyl-carbodiimide; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; mineral oil;
