1-trityl-4-((E)-3-(tert-butyldimethylsilyloxy)prop-1-enyl)-1H-imidazole

Base Information

• Chemical Name: 1-trityl-4-((E)-3-(tert-butyldimethylsilyloxy)prop-1-enyl)-1H-imidazole
• CAS No.: 1208244-25-0
• Molecular Formula: C₃₁H₃₆N₂OSi
• Molecular Weight: 480.725

Synonyms:1-trityl-4-((E)-3-(tert-butyldimethylsilyloxy)prop-1-enyl)-1H-imidazole

Chemical Property of 1-trityl-4-((E)-3-(tert-butyldimethylsilyloxy)prop-1-enyl)-1H-imidazole

Chemical Property:

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Technology Process of 1-trityl-4-((E)-3-(tert-butyldimethylsilyloxy)prop-1-enyl)-1H-imidazole

There total 1 articles about 1-trityl-4-((E)-3-(tert-butyldimethylsilyloxy)prop-1-enyl)-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

tert-butyldimethylsilyl chloride (18162-48-6) + 1-(triphenylmethyl)-4-(3-hydroxyprop-1-enyl)imidazole (138408-37-4) → 1-trityl-4-((E)-3-(tert-butyldimethylsilyloxy)prop-1-enyl)-1H-imidazole (1208244-25-0)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 0 - 25 ℃; for 1h;

DOI:10.1021/np900638e

Reference yield: 94.0%

1-trityl-4-((E)-3-(tert-butyldimethylsilyloxy)prop-1-enyl)-1H-imidazole (1208244-25-0) → C31H35N5OSi (1208244-26-1)

Guidance literature:

1-trityl-4-((E)-3-(tert-butyldimethylsilyloxy)prop-1-enyl)-1H-imidazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃;

With p-tosyldiazomethane; In tetrahydrofuran; hexane; at -78 ℃;

DOI:10.1021/np900638e

Reference yield: 63.0%

N-phenyl-maleimide (941-69-5) + 1-trityl-4-((E)-3-(tert-butyldimethylsilyloxy)prop-1-enyl)-1H-imidazole (1208244-25-0) → C41H43N3O3Si + (5SR,5aSR,8aSR)-5-((tert-butyldimethylsilyloxy)methyl)-8a-((RS)-2,5-dioxo-1-phenylpyrrolidin-3-yl)-7-phenyl-3-trityl-5,5a,7,8a-tetrahydroimidazo[4,5-e]isoindole-6,8(3H,4H)-dione

Guidance literature:

In toluene; at 110 ℃; for 20h;

DOI:10.1021/jo100416c

upstream raw materials:

tert-butyldimethylsilyl chloride

1-(triphenylmethyl)-4-(3-hydroxyprop-1-enyl)imidazole

Downstream raw materials:

C₃₁H₃₅N₅OSi

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