3-nitrobenzenesulfinic acid

Base Information

• Chemical Name: 3-nitrobenzenesulfinic acid
• CAS No.: 13257-95-9
• Molecular Formula: C₆H₅NO₄S
• Molecular Weight: 187.176

Synonyms:3-nitrobenzenesulfinic acid

Chemical Property of 3-nitrobenzenesulfinic acid

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

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MSDS Files:

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Technology Process of 3-nitrobenzenesulfinic acid

There total 9 articles about 3-nitrobenzenesulfinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

N-phenyl N-(3-nitrophenylsulfonyl) hydroxylamine (32234-30-3) → 3-nitrobenzenesulfinic acid (13257-95-9)

Guidance literature:

With sodium hydroxide; In diethyl ether;

Reference yield:

3-nitro-benzenethiosulfonic acid S-(3-nitro-phenyl ester) (38045-50-0) → bis(3-nitrophenyl) disulfide (537-91-7) + 3-nitrobenzenesulfinic acid (13257-95-9)

Guidance literature:

With aqueous alkali;

Reference yield:

3-Nitro-benzenesulfinic acid 1-phenyl-meth-(E)-ylideneamide → 3-nitrobenzenesulfinic acid (13257-95-9)

Guidance literature:

With water; In tetrahydrofuran; Heating;

DOI:10.1021/ja00477a045

upstream raw materials:

3-nitro-benzenethiosulfonic acid S-(3-nitro-phenyl ester)

3-nitro-aniline

N-phenyl N-(3-nitrophenylsulfonyl) hydroxylamine

nitrobenzene

Downstream raw materials:

3-nitro-benzenethiosulfonic acid S-(3-nitro-phenyl ester)

3-Nitrobenzenesulfonic acid

m-Nitro-benzolsulfonyl-trichlormethyl-disulfid

ethyl m-nitrobenzenesulphinate

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