(5S,1''R,2''S)-5-(4'-<2'',3''-dihydroxy-1''-methylpropyl>phenyl)-2-cyclohexenone

Base Information

Chemical Name:(5S,1''R,2''S)-5-(4'-<2'',3''-dihydroxy-1''-methylpropyl>phenyl)-2-cyclohexenone
CAS No.:174955-26-1
Molecular Formula:C₁₆H₂₀O₃
Molecular Weight:260.333
Hs Code.:

Synonyms:(5S,1''R,2''S)-5-(4'-<2'',3''-dihydroxy-1''-methylpropyl>phenyl)-2-cyclohexenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5S,1''R,2''S)-5-(4'-<2'',3''-dihydroxy-1''-methylpropyl>phenyl)-2-cyclohexenone

Chemical Property:

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Technology Process of (5S,1''R,2''S)-5-(4'-<2'',3''-dihydroxy-1''-methylpropyl>phenyl)-2-cyclohexenone

There total 1 articles about (5S,1''R,2''S)-5-(4'-<2'',3''-dihydroxy-1''-methylpropyl>phenyl)-2-cyclohexenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 174955-24-9
(3R,5S,1'R,4''S)-3-(4-<1'-<2'',2''-dimethyl-1,3-dioxolan-4''-yl>ethyl>phenyl)-5-(trimethylsilyl)cyclohexanone

: 174955-26-1
(5S,1''R,2''S)-5-(4'-<2'',3''-dihydroxy-1''-methylpropyl>phenyl)-2-cyclohexenone

Guidance literature:: With hydrogenchloride; copper dichloride; Yield given. Multistep reaction; 1.) DMF, 70 deg C, 30 min, 2.) MeOH, RT, 3 h;
DOI:10.1016/0957-4166(95)00443-2

Reference yield: 70.0%

: 174955-26-1
(5S,1''R,2''S)-5-(4'-<2'',3''-dihydroxy-1''-methylpropyl>phenyl)-2-cyclohexenone

: (5S,1''R,2''S)-3-(4'-<2'',3''-dihydroxy-1''-methylpropyl>phenyl)cyclohexanone

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 1.5h;
DOI:10.1016/0957-4166(95)00443-2

Reference yield:

: 174955-26-1
(5S,1''R,2''S)-5-(4'-<2'',3''-dihydroxy-1''-methylpropyl>phenyl)-2-cyclohexenone

: (2R,1''S)-2-(4'-<3''-oxocyclohexyl>phenyl)propanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / H₂ / Pd/C / ethyl acetate / 1.5 h

2: 82 percent / RuCl₃*H₂O, NaIO₄ / CCl₄; acetonitrile; H₂O / 1.25 h / Ambient temperature

With ruthenium trichloride; sodium periodate; hydrogen; palladium on activated charcoal; In tetrachloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1016/0957-4166(95)00443-2