C₂₇H₃₅N₇O₂

Base Information

• Chemical Name: C₂₇H₃₅N₇O₂
• CAS No.: 1638098-22-2
• Molecular Formula: C₂₇H₃₅N₇O₂
• Molecular Weight: 489.621
• Mol file: 1638098-22-2.mol

Synonyms:C₂₇H₃₅N₇O₂

Chemical Property of C₂₇H₃₅N₇O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₃₅N₇O₂

There total 5 articles about C₂₇H₃₅N₇O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C37H55N7O4 (1638098-21-1) → C27H35N7O2 (1638098-22-2)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 2h; pH=2;

DOI:10.1002/chem.201400365

Reference yield:

1-azidomethyl-3,5-bis(trifluoroacetamidomethyl)-2,4,6-triethylbenzene (1638098-17-5) → C27H35N7O2 (1638098-22-2)

Guidance literature:

Multi-step reaction with 4 steps

1: water; sodium hydroxide / methanol / 20 °C

2: acetic acid / chloroform / 20 °C

3: sodium tetrahydroborate / chloroform; methanol / 1 h / 0 - 20 °C

4: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C / pH 2

With hydrogenchloride; sodium tetrahydroborate; water; acetic acid; sodium hydroxide; In tetrahydrofuran; methanol; chloroform; water;

DOI:10.1002/chem.201400365

Reference yield:

[3,5-bis(bromomethyl)-2,4,6-triethylphenyl]methyl azide (259268-22-9) → C27H35N7O2 (1638098-22-2)

Guidance literature:

Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.08 h / 0 °C

1.2: 20 °C

2.1: water; sodium hydroxide / methanol / 20 °C

3.1: acetic acid / chloroform / 20 °C

4.1: sodium tetrahydroborate / chloroform; methanol / 1 h / 0 - 20 °C

5.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C / pH 2

With hydrogenchloride; sodium tetrahydroborate; water; sodium hydride; acetic acid; sodium hydroxide; In tetrahydrofuran; methanol; chloroform; water; N,N-dimethyl-formamide; mineral oil;

DOI:10.1002/chem.201400365

upstream raw materials:

1,3-bis(aminomethyl)-5-azidomethyl-2,4,6-triethylbenzene

C₃₇H₅₅N₇O₄

[3,5-bis(bromomethyl)-2,4,6-triethylphenyl]methyl azide

1-azidomethyl-3,5-bis(trifluoroacetamidomethyl)-2,4,6-triethylbenzene