(2S,3R)-benzyl 2-(N-2-nitrobenzenesulfonyl-N-methyl)amino-3-((triisopropylsilyl)-oxy)butanoate

Base Information

Chemical Name:(2S,3R)-benzyl 2-(N-2-nitrobenzenesulfonyl-N-methyl)amino-3-((triisopropylsilyl)-oxy)butanoate
CAS No.:1426250-03-4
Molecular Formula:C₂₇H₄₀N₂O₇SSi
Molecular Weight:564.775
Hs Code.:

Synonyms:(2S,3R)-benzyl 2-(N-2-nitrobenzenesulfonyl-N-methyl)amino-3-((triisopropylsilyl)-oxy)butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-benzyl 2-(N-2-nitrobenzenesulfonyl-N-methyl)amino-3-((triisopropylsilyl)-oxy)butanoate

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Technology Process of (2S,3R)-benzyl 2-(N-2-nitrobenzenesulfonyl-N-methyl)amino-3-((triisopropylsilyl)-oxy)butanoate

There total 6 articles about (2S,3R)-benzyl 2-(N-2-nitrobenzenesulfonyl-N-methyl)amino-3-((triisopropylsilyl)-oxy)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353655-05-6
(2S,3R)-benzyl 2-(2-nitrobenzenesulfonyl)amino-3-((triisopropylsilyl)oxy)butanoate

: 74-88-4
methyl iodide

: 1426250-03-4
(2S,3R)-benzyl 2-(N-2-nitrobenzenesulfonyl-N-methyl)amino-3-((triisopropylsilyl)-oxy)butanoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2011.10.099

Reference yield:

: 1353654-65-5
(2S,3R)-benzyl 2-amino-3-((triisopropylsilyl)oxy)butanoate

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 1426250-03-4
(2S,3R)-benzyl 2-(N-2-nitrobenzenesulfonyl-N-methyl)amino-3-((triisopropylsilyl)-oxy)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.10.099

Reference yield:

: 1353655-04-5
C₃₅H₄₅NO₅Si

: 1426250-03-4
(2S,3R)-benzyl 2-(N-2-nitrobenzenesulfonyl-N-methyl)amino-3-((triisopropylsilyl)-oxy)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With piperidine; potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.10.099