[1-(4,4'-dimethoxytrityl)]-(3-D,L-α-tocopheryl)glycerol-2-phosphoramidite

Base Information

Chemical Name:[1-(4,4'-dimethoxytrityl)]-(3-D,L-α-tocopheryl)glycerol-2-phosphoramidite
CAS No.:850544-45-5
Molecular Formula:C₆₂H₉₁N₂O₇P
Molecular Weight:1007.39
Hs Code.:

Synonyms:[1-(4,4'-dimethoxytrityl)]-(3-D,L-α-tocopheryl)glycerol-2-phosphoramidite

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1-(4,4'-dimethoxytrityl)]-(3-D,L-α-tocopheryl)glycerol-2-phosphoramidite

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Technology Process of [1-(4,4'-dimethoxytrityl)]-(3-D,L-α-tocopheryl)glycerol-2-phosphoramidite

There total 3 articles about [1-(4,4'-dimethoxytrityl)]-(3-D,L-α-tocopheryl)glycerol-2-phosphoramidite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.4%

: 124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

: 142386-80-9
[1-(4,4'-dimethoxytrityl)]-3-D,L-α-tocopherylglycerol

: 850544-45-5
[1-(4,4'-dimethoxytrityl)]-(3-D,L-α-tocopheryl)glycerol-2-phosphoramidite

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 142386-77-4
2,3-isopropylidene-1-D,L-α-tocopherolglycerol

: 850544-45-5
[1-(4,4'-dimethoxytrityl)]-(3-D,L-α-tocopheryl)glycerol-2-phosphoramidite

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; water / tetrahydrofuran / 2 h / 20 °C / Darkness

2: pyridine / 12 h / 20 °C / Darkness

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 142386-79-6
1-D,L-α-tocopherylglycerol

: 850544-45-5
[1-(4,4'-dimethoxytrityl)]-(3-D,L-α-tocopheryl)glycerol-2-phosphoramidite

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 12 h / 20 °C / Darkness

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

With pyridine; N-ethyl-N,N-diisopropylamine; In dichloromethane;